Simultaneous determination of biogenic amines and estrogens in foodstuff by an improved HPLC method combining with fluorescence labeling

被引：36
|
作者：
Li, Guoliang [1 ]
Dong, Lihua [3 ]
Wang, Aihong [2 ]
Wang, Wenli [1 ]
Hu, Na [2 ]
You, Jinmao [1 ,2 ]
机构：
[1] Qufu Normal Univ, Key Lab Life Organ Anal Shandong Prov, Qufu, Peoples R China
[2] Chinese Acad Sci, Northwest Inst Plateau Biol, Key Lab Tibetan Med Res, Xining, Peoples R China
[3] Taishan Med Univ, Sch Chem Engn, Tai An, Shandong, Peoples R China
来源：
LWT-FOOD SCIENCE AND TECHNOLOGY | 2014年 / 55卷 / 01期
基金：
美国国家科学基金会;
关键词：
HPLC analysis; Foodstuff; Biogenic amines; Estrogens; Fluorescence labeling; PERFORMANCE LIQUID-CHROMATOGRAPHY; PRECOLUMN DERIVATIZATION; MASS-SPECTROMETRY; FOOD; EXTRACTION; TISSUES; KIDNEY; URINE; MILK; MEAT;
D O I：
10.1016/j.lwt.2013.06.028
中图分类号：
TS2 [食品工业];
学科分类号：
0832 ;
摘要：
Biogenic amines (BA) and estrogens (ES) have attracted increasing attentions due to their significance on food safety and food quality. In this study, a novel HPLC-FLD method using ethyl-acridine-sulfonyl chloride (EAC) as fluorescence labeling reagent has been developed for simultaneous determination of BA and ES in food samples. The labeling conditions including labeling time, pH of borate buffers and amount of EAC were optimized. The simultaneous labeling of BA and ES can be finished in as little as 6 min. This method without complex pre-treatment offered the low LOD of 0.27-0.69 ng/mL. It was applied to analyze several food samples (beer, cheese, fish, sausage and shrimp), and showed excellent applicability. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码：355 / 361
页数：7
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