Structure of MCM-48 revealed by transmission electron microscopy

被引:247
作者
Alfredsson, V
Anderson, MW
机构
[1] Department of Chemistry, UMIST, Manchester M60 1QD
关键词
D O I
10.1021/cm950568k
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A model of the cubic mesoporous silicate MCM-48, based on the gyroid minimal surface, has been generated by computer simulation. Transmission electron micrographs and X-ray diffraction (XRD) patterns have been recorded for MCM-48 and compared with the images and XRD patterns obtained by modeling. The gyroid minimal surface gives an excellent description for the structure of MCM-48 with the amorphous hydroxylated silicate sited close to the midplane of the surface.
引用
收藏
页码:1141 / 1146
页数:6
相关论文
共 21 条
[1]   THE INTRINSIC CURVATURE OF SOLIDS [J].
ANDERSSON, S ;
HYDE, ST ;
VONSCHNERING, HG .
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1984, 168 (1-4) :1-17
[2]   MINIMAL-SURFACES AND STRUCTURES - FROM INORGANIC AND METAL CRYSTALS TO CELL-MEMBRANES AND BIO-POLYMERS [J].
ANDERSSON, S ;
HYDE, ST ;
LARSSON, K ;
LIDIN, S .
CHEMICAL REVIEWS, 1988, 88 (01) :221-242
[3]   X-RAY-DIFFRACTION STUDY OF MESOPHASES OF CETYLTRIMETHYLAMMONIUM BROMIDE IN WATER, FORMAMIDE, AND GLYCEROL [J].
AUVRAY, X ;
PETIPAS, C ;
ANTHORE, R ;
RICO, I ;
LATTES, A .
JOURNAL OF PHYSICAL CHEMISTRY, 1989, 93 (21) :7458-7464
[4]  
BECK JS, 1992, J AM CHEM SOC, V114, P10835
[5]  
CARLSSON A, 1992, ELECTRON MICROS, V1, P497
[6]   X-RAY DIFFRACTION STUDIES OF ECHINODERM PLATES [J].
DONNAY, G ;
PAWSON, DL .
SCIENCE, 1969, 166 (3909) :1147-&
[7]   ACCURATE ATOMIC POSITIONS FROM ELECTRON-MICROSCOPY [J].
HOVMOLLER, S ;
SJOGREN, A ;
FARRANTS, G ;
SUNDBERG, M ;
MARINDER, BO .
NATURE, 1984, 311 (5983) :238-241
[8]   GENERALIZED SYNTHESIS OF PERIODIC SURFACTANT INORGANIC COMPOSITE-MATERIALS [J].
HUO, QS ;
MARGOLESE, DI ;
CIESLA, U ;
FENG, PY ;
GIER, TE ;
SIEGER, P ;
LEON, R ;
PETROFF, PM ;
SCHUTH, F ;
STUCKY, GD .
NATURE, 1994, 368 (6469) :317-321
[9]   MESOSTRUCTURE DESIGN WITH GEMINI SURFACTANTS - SUPERCAGE FORMATION IN A 3-DIMENSIONAL HEXAGONAL ARRAY [J].
HUO, QS ;
LEON, R ;
PETROFF, PM ;
STUCKY, GD .
SCIENCE, 1995, 268 (5215) :1324-1327
[10]   ORGANIZATION OF ORGANIC-MOLECULES WITH INORGANIC MOLECULAR-SPECIES INTO NANOCOMPOSITE BIPHASE ARRAYS [J].
HUO, QS ;
MARGOLESE, DI ;
CIESLA, U ;
DEMUTH, DG ;
FENG, PY ;
GIER, TE ;
SIEGER, P ;
FIROUZI, A ;
CHMELKA, BF ;
SCHUTH, F ;
STUCKY, GD .
CHEMISTRY OF MATERIALS, 1994, 6 (08) :1176-1191