Preparation and characterization of mucilage polysaccharide for biomedical applications

被引:131
作者
Archana, G. [1 ]
Sabina, K. [1 ]
Babuskin, S. [1 ]
Radhakrishnan, K. [1 ]
Fayidh, Mohammed A. [1 ]
Babu, P. Azhagu Saravana [1 ]
Sivarajan, M. [2 ]
Sukumar, M. [1 ]
机构
[1] Anna Univ, AC Tech, Ctr Biotechnol, Madras 600025, Tamil Nadu, India
[2] Cent Leather Res Inst, Div Chem Engn, Madras 20, Tamil Nadu, India
关键词
Carbohydrates; Polysaccharide; Swelling index; Emulsifying capacity; Abelmoscus esculentus; Gracilaria corticata; STRUCTURAL-CHARACTERIZATION; OKRA MUCILAGE; FILMS; CHITOSAN; FRACTION;
D O I
10.1016/j.carbpol.2013.04.062
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
In the present investigation, the polysaccharide/mucilage from waste of Abelmoscus esculentus by modification in hot extraction using two different solvents (Acetone, Methanol) were extracted, characterized and further compared with seaweed polysaccharide for their potential applications. The percentage yield, emulsifying capacity and swelling index of this mucilage were determined. The macro algae and okra waste, gave high % yield (22.2% and 8.6% respectively) and good emulsifying capacity (EC% = 52.38% and 54.76% respectively) with acetone, compared to methanol (11.3% and 0.28%; EC% = 50%) (PH = 7) while swelling index was greater with methanol than acetone extracts respectively. The infrared (I.R.) spectrum of the samples was recorded to investigate the chemical structure of mucilage. Thermal analysis of the mucilage was done with TGA (Thermal Gravimetric Analyzer) and DSC (Differential Scanning Calorimeter) which showed both okra and algal polysaccharide were thermostable hydrogels. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:89 / 94
页数:6
相关论文
共 30 条
[1]  
Al-Barak A. B. S., 2010, Research Journal of Environmental Sciences, V4, P566
[2]   Extraction and physico-chemical characterization of a versatile biodegradable polysaccharide obtained from green algae [J].
Alves, Anabela ;
Caridade, Sofia G. ;
Mano, Joao F. ;
Sousa, Rui A. ;
Reis, Rui L. .
CARBOHYDRATE RESEARCH, 2010, 345 (15) :2194-2200
[3]   Effect of Different Purification Techniques on the Characteristics of Heteropolysaccharide-Protein Biopolymer from Durian (Durio zibethinus) Seed [J].
Amid, Bahareh Tabatabaee ;
Mirhosseini, Hamed .
MOLECULES, 2012, 17 (09) :10875-10892
[4]   Fractionation of extracted Madagascan Gracilaria corticata polysaccharides:: Structure and properties [J].
Andriamanantoanina, H. ;
Chambat, G. ;
Rinaudo, M. .
CARBOHYDRATE POLYMERS, 2007, 68 (01) :77-88
[5]   WORLDWIDE USE AND IMPORTANCE OF GRACILARIA [J].
ARMISEN, R .
JOURNAL OF APPLIED PHYCOLOGY, 1995, 7 (03) :231-243
[6]   Structural characterization of polysaccharide obtained from red seaweed Gracilaria caudata (J Agardh) [J].
Barros, Francisco C. N. ;
da Silva, Draulio C. ;
Sombra, Venicios G. ;
Maciel, Jeanny S. ;
Feitosa, Judith P. A. ;
Freitas, Ana L. P. ;
de Paula, Regina C. M. .
CARBOHYDRATE POLYMERS, 2013, 92 (01) :598-603
[7]   Biological properties of the chitosan-gelatin sponge wound dressing [J].
Deng, Chun-Mei ;
He, Lan-Zhen ;
Zhao, Ming ;
Yang, Dan ;
Liu, Yi .
CARBOHYDRATE POLYMERS, 2007, 69 (03) :583-589
[8]  
Distantina S., 2011, ENG TECHNOLOGY, V54, P738
[9]  
Fan Y., 2011, CARBOHYD POLYM, V85, P157
[10]  
Fernandez J. P., 2003, ANAL CHIM ACTA, V480, P23