Increase in the Mechanical Strength of Mg-8Gd-3Y-1Zn Alloy Containing Long-Period Stacking Ordered Phases Using Equal Channel Angular Pressing Processing

被引:18
作者
Garces, Gerardo [1 ]
Perez, Pablo [1 ]
Barea, Rafael [2 ]
Medina, Judit [1 ]
Stark, Andreas [3 ]
Schell, Norbert [4 ]
Adeva, Paloma [1 ]
机构
[1] CSIC, CENIM, Ctr Nacl Invest Met, Dept Met Fis, Avda Gregorio del Amo 8, Madrid 28040, Spain
[2] Univ Nebrija, Dept Ingn Ind, Campus Dehesa de la Villa,C Pirineos 55, Madrid 28040, Spain
[3] Helmholtz Zentrum Geesthacht, Inst Mat Res, Max Planck Str 1, D-21502 Geesthacht, Germany
[4] Helmholtz Zentrum Geesthacht, Struct Res New Mat, DESY, Notkestr 85, D-22607 Hamburg, Germany
关键词
magnesium alloys; LPSO; ECAP; precipitation; ZN-ZR ALLOY; MICROSTRUCTURE EVOLUTION; LPSO PHASE; GD ALLOY; EXTRUSION; DEFORMATION; TEMPERATURE; COMBINATION; TEXTURE; STRAIN;
D O I
10.3390/met9020221
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The evolution of the microstructure and mechanical properties during equal channel angular pressing processing has been studied in an extruded Mg-Gd-Y-Zn alloy containing long-period stacking ordered phases. After extrusion, the microstructure is characterized by the presence of long-period stacking ordered fibers elongated along the extrusion direction within the magnesium matrix. The grain structure is a mixture of randomly oriented dynamic recrystallized and coarse highly oriented non-dynamic recrystallized grains. Rare-earth atoms are in solid solution after extrusion at 400 degrees C and precipitation takes place during the thermal treatment at 200 degrees C. Precipitation of beta' prismatic plates and lamellar gamma' in the basal plane increases the tensile yield stress from 325 to 409 MPa. During equal channel angular pressing processing at 300 degrees C, the volume fraction of dynamic recrystallized grains continuously increases with the strain introduced during the equal channel angular pressing process. Precipitation of beta phase is equally observed at grain boundaries of the ECAPed alloy. Dynamic recrystallized grain size decreases from 1.8 mu m in the extruded material to 0.5 mu m in the ECAPed alloy. Thermal treatment at 200 degrees C of ECAPed materials results in an increase of the yield stress up to 456 MPa, which is maintained up to 200 degrees C.
引用
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页数:17
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