Evaluation of Simulant Migration of Volatile Nitrosamines from Latex Gloves and Balloons by HS-SPME-GC-MS

被引：15

作者：

Feng, Di ^{[1
]}

Liu, Luo ^{[1
]}

Zhao, Liyuan ^{[1
]}

Zhou, Qingfeng ^{[1
]}

Tan, Tianwei ^{[1
]}

机构：

[1] Beijing Univ Chem Technol, Coll Life Sci & Technol, Beijing Key Lab Bioproc, Beijing, Peoples R China

来源：

JOURNAL OF CHROMATOGRAPHIC SCIENCE | 2012年 / 50卷 / 08期

基金：

国家高技术研究发展计划(863计划); 中国国家自然科学基金;

关键词：

SOLID-PHASE MICROEXTRACTION; N-NITROSAMINES; FOOD; RUBBER;

D O I：

10.1093/chromsci/bms057

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Nitrosamines are a group of carcinogens that have been found in various latex products. Methods have been developed for extraction, concentration and detection of simulant migration of volatile nitrosamines from latex gloves and balloons. After glove samples or balloon samples were treated with artificial sweat and artificial saliva, headspace solid-phase microextraction and gas chromatography with mass spectrometer detection were performed. Eight volatile nitrosamines were extracted by a fused silica fiber coated with carboxen-polydimethylsioxane, and solid-phase microextraction conditions were optimized. The developed method was successfully used to analyze simulant migration of volatile nitrosamines from latex gloves and balloons. The described methods are rapid and simple, with adequate sensitivity and without organic solvent.

引用

页码：733 / 738

页数：6

共 50 条

[31] Response surface optimization of SPME extraction conditions for the analysis of volatile compounds in Brazilian sugar cane spirits by HS-SPME-GC-MS [J].

Zacaroni, Lidiany Mendonca ;

de Sales, Priscila Ferreira ;

Cardoso, Maria das Gracas ;

Santiago, Wilder Douglas ;

Nelson, David Lee .

JOURNAL OF THE INSTITUTE OF BREWING, 2017, 123 (02) :226-231

[32] Determination of terpene alcohols in Sicilian Muscat wines by HS-SPME-GC-MS [J].

Barbera, Daniela ;

Avellone, Giuseppe ;

Filizzola, Felice ;

Monte, Lucio G. ;

Catanzaro, Paola ;

Agozzino, Pasquale .

NATURAL PRODUCT RESEARCH, 2013, 27 (06) :541-547

[33] HS-SPME-GC-MS for the Quantitation and Chiral Characterization of Camphor and Menthol in Creams [J].

Fiori, Jessica ;

Naldi, Marina ;

Gotti, Roberto .

CHROMATOGRAPHIA, 2010, 72 (9-10) :941-947

[34] Decoding carob flavor aroma using HS-SPME-GC-MS and chemometrics [J].

Krokou, Andriana ;

Kokkinofta, Rebecca ;

Stylianou, Marinos ;

Agapiou, Agapios .

EUROPEAN FOOD RESEARCH AND TECHNOLOGY, 2020, 246 (07) :1419-1428

[35] Differentiation and characterization of volatile compounds in five common milk powders using HS-GC-IMS, HS-SPME-GC-MS, and multivariate statistical approaches [J].

Zhou, Yaxi ;

Wang, Diandian ;

Zhao, Jian ;

Guo, Yu ;

Yan, Wenjie .

FOOD CHEMISTRY-X, 2025, 25

[36] Effect of hot air drying on volatile compounds of Flammulina velutipes detected by HS-SPME-GC-MS and electronic nose [J].

Yang, Wenjian ;

Yu, Jie ;

Pei, Fei ;

Mariga, Alfred Mugambi ;

Ma, Ning ;

Fang, Yong ;

Hu, Qiuhui .

FOOD CHEMISTRY, 2016, 196 :860-866

[37] Characterization of Volatile Organic Compounds (VOCs) from Farms Effluents: Interest of HS-SPME-GC-MS Technique for Laboratory and Field Test [J].

Joguet, Nicolas ;

Jing, Lun ;

Jamois, Frank ;

Dumargue, Philippe .

ATMOSPHERE, 2023, 14 (06)

[38] HS-SPME-GC-MS Analysis of the Volatile Composition of Italian Honey for Its Characterization and Authentication Using the Genetic Algorithm [J].

Breschi, Carlotta ;

Ieri, Francesca ;

Calamai, Luca ;

Miele, Alessandra ;

D'Agostino, Silvia ;

Melani, Fabrizio ;

Zanoni, Bruno ;

Mulinacci, Nadia ;

Cecchi, Lorenzo .

SEPARATIONS, 2024, 11 (09)

[39] Profiling of Volatile Compounds in 'Muscat Hamburg' Contaminated with Aspergillus carbonarius before OTA Biosynthesis Based on HS-SPME-GC-MS and DLLME-GC-MS [J].

Guo, Yayun ;

Wang, Zhe ;

He, Yi ;

Gao, Huanhuan ;

Shi, Hongmei .

MOLECULES, 2024, 29 (03)

[40] Quantification of Polyfunctional Thiols in Wine by HS-SPME-GC-MS Following Extractive Alkylation [J].

Musumeci, Lauren E. ;

Ryona, Imelda ;

Pan, Bruce S. ;

Loscos, Natalia ;

Feng, Hui ;

Cleary, Michael T. ;

Sacks, Gavin L. .

MOLECULES, 2015, 20 (07) :12280-12299

← 1 2 3 4 5 →