Synthesis of 1,3-bis(4,5-dihydrothiazole) benzene

被引：0
|
作者：
Atwood, D. A. [1 ]
Delcamp, J. [1 ]
Zaman, M. K. [1 ]
机构：
[1] Univ Kentucky, Lexington, KY 40506 USA
来源：
MAIN GROUP CHEMISTRY | 2006年 / 5卷 / 02期
关键词：
BDETH2; Trimethylaluminum; Cyclization;
D O I：
10.1080/10241220600888350
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new compound, 1,3-bis(4,5-dihydrothiazole) benzene was synthesized by refluxing benzene-1,3-diamidoethanethiol (BDETH2) in toluene in the presence of trimethylaluminum. The compound was characterized by IR, NMR, Mass spectroscopy, Elemental Analysis, and X-ray crystallography.
引用
收藏
页码：137 / 140
页数：4
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