Synthesis and Crystal Structure of 4,4′,6,6′-Tetrachloro-2,2′-[(1,4-butylene)dioxybis(nitrilmethylidyne)]diphenol

被引：1
|
作者：
Wang, Li [1 ]
Dong, Xiu-Yan [1 ]
Zhao, Li [1 ]
Yang, Yu-Hua [1 ]
机构：
[1] Lanzhou Jiaotong Univ, Sch Chem & Biol Engn, Lanzhou 730070, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2013年 / 25卷 / 06期
关键词：
Salen-type bisoxime compound; Synthesis; Crystal structure; Supramolecular interaction; COMPLEXES;
D O I：
10.14233/ajchem.2013.13920A
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The compound 4,4',6,6'-tetrachloro-2,2'-[(1,4-bytylene)dioxybis(nitrilmethylidyne)]diphenol with the molecular formula C18H16Cl4N2O4, was synthesized by the reaction of 3,5-dichloro-2-hydroxybenzaldehyde with 1,4-bis(aminooxy)butane in ethanol. The molecule is disposed about a crystallographic centre of symmetry and the molecule adopts an extended conformation where the two phenoldoxime moieties are aparat from each other. There are strong O-H center dot center dot center dot N intramolecular hydrogen bond and weak C-H center dot center dot center dot O and C-H center dot center dot center dot Cl intermolecular hydrogen bonds and strong intermolecular stacking interactions (the nearest benzene rings are parallel to that of another molecule are ca 2.512(2) angstrom, stabilizing the two dimensional structures of the present compound.
引用
收藏
页码：3440 / 3442
页数：3
相关论文
共 50 条
  • [41] Lanthanide coordination compounds with 2,2′-bipyridine-6,6′-dicarboxylate: Synthesis, crystal structure, luminescence and magnetic property
    Ren, Ya-Lan
    Wang, Fei
    Hu, Huai-Ming
    Chang, Zhuguo
    Yang, Meng-Lin
    Xue, Ganglin
    INORGANICA CHIMICA ACTA, 2015, 434 : 104 - 112
  • [42] (4,4′,6,6′-Tetra-tert-butyl-2,2′-{[2-(dimethylamino)ethyl]nitrilobis(methylene)}diphenolato)dioxidomolybdenum(VI) chloroform monosolvate
    Lei, Xiangyang
    Chelamalla, Nagasree
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M1510 - +
  • [43] Bis(2-phenylpyridinato,-C2′,N)[4,4′-bis(4-Fluorophenyl)-6,6′-dimethyl-2,2′-bipyridine] Iridium(III) Hexafluorophosphate
    Glykos, Dimitrios
    Plakatouras, John C.
    Malandrinos, Gerasimos
    MOLBANK, 2023, 2023 (02)
  • [44] Synthesis and Characterization of a New 3D Pillared Bilayer Cd(II) Coordination Polymer Based on 6,6′-Dinitro-2,2′,4,4′-biphenyltetracarboxylic Acid
    Wang Ji-Wu
    Su Yong-Chao
    Wang Ji-Jiang
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2015, 34 (09) : 1385 - 1390
  • [45] Synthesis, Crystal Structure and Photoluminescence of a Zn(Ⅱ) Coordination Polymer Derived from 1,1'-Biphenyl-2,2',6,6'-tetracarboxylic Acid
    弓亚琼
    米陶清
    江飞龙
    结构化学, 2015, 34 (07) : 1087 - 1091
  • [46] Synthesis and crystal structure of erbium nitrate complex with 6,6'-bis(diphenylphosphine oxide methyl)-2,2'-bipyridine-1,1'-dioxide
    Feng, YC
    Tang, Y
    Tang, N
    Gan, XM
    Tan, MY
    Yu, KB
    CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 1996, 17 (11): : 1678 - 1681
  • [47] 4,4′,4"-Trimethy1-2,2′:6′,2"-terpyridine by Oxidative Coupling of 4-Pico line
    Robo, Michael T.
    Prinsell, Michael R.
    Weix, Daniel J.
    JOURNAL OF ORGANIC CHEMISTRY, 2014, 79 (21) : 10624 - 10628
  • [48] Hydrothermal synthesis and crystal structure of new coordination polymers with 2,2′-bipyridine-4,4′-dicarboxylic acid
    Yan, Shaohua
    Zheng, Xiangjun
    JOURNAL OF MOLECULAR STRUCTURE, 2010, 964 (1-3) : 52 - 57
  • [49] Hydrothermal Synthesis and Crystal Structure of 1D Zigzag Chain [Zn(Hbsal)2(4,4′-bipy)]n
    Jiang, Xiu-Rong
    Wen, De-Cai
    Dong, Yan
    Chen, Wu-Hua
    ASIAN JOURNAL OF CHEMISTRY, 2011, 23 (06) : 2821 - 2822
  • [50] Synthesis, crystal structure and magnetic property of a Ni(II) complex with 4′-(4-methoxyphenyl)-2,2′:6′,2"-terpyridine
    Fu, Wei-Wei
    Shen, Jing-Run
    Tang, Zi-Qing
    Peng, Yong-Qiong
    Yi, Qing
    INORGANIC AND NANO-METAL CHEMISTRY, 2017, 47 (12) : 1664 - 1667
12345