Synthesis and Characterization of Anatase Titanium Dioxide Nanoparticles Using Egg White Solution via Sol-Gel Method

被引:179
作者
Bagheri, Samira [1 ]
Shameli, Kamyar [1 ,2 ]
Abd Hamid, Sharifah Bee [1 ]
机构
[1] Univ Malaya, Ctr Res Nanotechnol & Catalysis NANOCEN, Kuala Lumpur 50603, Malaysia
[2] Univ Putra Malaysia, Fac Sci, Dept Chem, Serdang 43400, Selangor, Malaysia
关键词
TIO2; HYDROLYSIS;
D O I
10.1155/2013/848205
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Anatase titanium dioxide nanoparticles (TNPs) are synthesized by a simple and cost-effective process with and without freshly water-soluble egg white proteins (albumin) via sol-gel method. The main advantage of using egg white proteins as a gelling agent is that it can provide long-term stability for nanoparticles by preventing particles agglomeration. The X-ray diffraction and FTIR results indicate that the synthesized nanoparticles have only the anatase structure without the presence of any other phase impurities. Additionally, the TNPs are characterized by a number of techniques such as thermogravimetric analysis (TGA), X-ray diffraction analysis (XRD), transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), and ultraviolet visible spectra (UV-vis). The sizes of titanium dioxide nanoparticles with and without using egg white solution are 12.55 +/- 3.42 nm and 21.45 +/- 4.21 nm, respectively. The results indicate that egg white solution is a reliable and cheap green gelling agent that can be used as a matrix in the sol-gel method to synthesis tiny size TNPs.
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页数:5
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