Ceramic montmorillonite nanocomposites by electrochemical synthesis

被引:21
作者
Wang, Adele Qi [1 ]
D'Souza, Nandika [2 ]
Golden, Teresa Diane [1 ]
机构
[1] Univ N Texas, Dept Chem, Denton, TX 76203 USA
[2] Univ N Texas, Dept Mat Sci, Denton, TX 76203 USA
关键词
Montmorillonite; Nanocomposites; Ceramics;
D O I
10.1016/j.clay.2008.02.004
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Nanocomposite powders of montmorillonite and cerium oxide are synthesized using an electrochemical technique. X-ray diffraction of the nanocomposites shows a random orientation of the powders with particle sizes as small as 4-6 nm. The montmorillonite percentage in the nanocomposite is also shown to affect sintering rates and particle size growth as shown by X-ray diffraction. Fourier transmission infrared measurements confirm the presence of individual platelets of the montmorillonite within the nanocomposite matrix. Nanocomposites containing 1% of the montmorillonite in the matrix increase crystallization, while higher percentages of montmorillonite inhibit particle growth during sintering. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:310 / 317
页数:8
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