Characterization of electrochemically etched tungsten tips for scanning tunneling microscopy

被引:1
作者
Müller, AD [1 ]
Müller, F
Hietschold, M
Demming, F
Jersch, J
Dickmann, K
机构
[1] Univ Chemnitz, Inst Phys, D-09107 Chemnitz, Germany
[2] Laserzentrum FH Munster, D-48565 Steinfurt, Germany
关键词
D O I
暂无
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Shape and composition of electrochemically etched tungsten tips for use in scanning tunneling microscopy (STM) were investigated in a transmission electron microscope (TEM) with a Gathan imaging filter (GIP). The tips are prepared by a lamella drop-off technique. We observe typical tip radii of less than 10 nm. After a storage of some days under ambient conditions, an amorphous oxide film is detectable. The electron energy-loss spectroscopy confirms that the surface is contaminated by compounds that contain carbon, too. (C) 1999 American Institute of Physics. [S0034- 6748(99)01110-7].
引用
收藏
页码:3970 / 3972
页数:3
相关论文
共 9 条
[1]   ION MILLED TIPS FOR SCANNING TUNNELING MICROSCOPY [J].
BIEGELSEN, DK ;
PONCE, FA ;
TRAMONTANA, JC ;
KOCH, SM .
APPLIED PHYSICS LETTERS, 1987, 50 (11) :696-698
[2]   PREPARATION AND CHARACTERIZATION OF TUNGSTEN TIPS FOR SCANNING-TUNNELING-MICROSCOPY [J].
CRICENTI, A ;
PAPARAZZO, E ;
SCARSELLI, MA ;
MORETTO, L ;
SELCI, S .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1994, 65 (05) :1558-1560
[3]  
EKWALL I, 1999, MEAS SCI TECHNOL, V10, P11
[4]   A CONVENIENT METHOD FOR REMOVING SURFACE OXIDES FROM TUNGSTEN STM TIPS [J].
HOCKETT, LA ;
CREAGER, SE .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1993, 64 (01) :263-264
[5]   An improved lamellae drop-off technique for sharp tip preparation in scanning tunneling microscopy [J].
Klein, M ;
Schwitzgebel, G .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (08) :3099-3103
[6]   CHARACTERIZATION OF TUNGSTEN TIPS FOR STM BY SEM AES XPS [J].
LISOWSKI, W ;
VANDENBERG, AHJ ;
KIP, GAM ;
HANEKAMP, LJ .
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1991, 341 (3-4) :196-199
[7]  
OLIA AI, 1996, REV SCI INSTRUM, V67, P1917
[8]   Low thermal power electron beam annealing of scanning tunneling microscope tips [J].
Scholz, R ;
Agne, M ;
Breitenstein, O ;
Jenniches, H .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (08) :3262-3263
[9]   OXYGEN-INDUCED SHARPENING PROCESS OF W(111) TIPS FOR SCANNING TUNNELING MICROSCOPE USE [J].
WENGELNIK, H ;
NEDDERMEYER, H .
JOURNAL OF VACUUM SCIENCE & TECHNOLOGY A-VACUUM SURFACES AND FILMS, 1990, 8 (01) :438-440