Ti3SiC2-Cf composites by spark plasma sintering: Processing, microstructure and thermo-mechanical properties

被引:32
作者
Lagos, M. A. [1 ]
Pellegrini, C. [2 ]
Agote, I. [1 ]
Azurmendi, N. [1 ]
Barcena, J. [1 ]
Parco, M. [1 ]
Silvestroni, L. [3 ]
Zoli, L. [3 ]
Sciti, D. [3 ]
机构
[1] TECNALIA, Ind & Transport Div, Mikeletegi Pasealekua 2, E-20009 San Sebastian, Spain
[2] ENSCI, European Ceram Ctr, F-87100 Limoges, France
[3] CNR, Inst Sci & Technol Ceram, ISTEC, Via Granarolo 64, I-48018 Faenza, Italy
基金
欧盟地平线“2020”;
关键词
Ceramic matrix composites; Max phases; Interface; Mechanical properties; Sintering; SPS; Spark plasma sintering; MECHANICAL-PROPERTIES; TEMPERATURE; PHASE; FABRICATION; UHTCMCS;
D O I
10.1016/j.jeurceramsoc.2019.03.037
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
MAX phases, and particularly Ti3SiC2, are interesting for high temperature applications. The addition of carbon fibers can be used to reduce the density and to modify the properties of the matrix. This work presents the densification and characterization of Ti3SiC2 based composites with short carbon fibers using a fast and simple fabrication approach: dry mixing and densification by Spark Plasma Sintering. Good densification level was obtained below 1400 degrees C even with a high amount of fibers. The reaction of the fibers with the matrix is limited thanks to the fast processing time and depends on the amount of fibers in the composite. Bending strength at room temperature, between 437 and 120 MPa, is in the range of conventional CMCs with short fibers and according to the resistance of the matrix and the presence of residual porosity. Thermo-mechanical properties of the composites up to 1500 degrees C are also presented.
引用
收藏
页码:2824 / 2830
页数:7
相关论文
共 31 条
[1]  
Bao Y. W., 2004, ACTA METALL, V17, P465
[2]   Thermal properties of Ti3SiC2 [J].
Barsoum, MW ;
El-Raghy, T ;
Rawn, CJ ;
Porter, WD ;
Wang, H ;
Payzant, EA ;
Hubbard, CR .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1999, 60 (04) :429-439
[3]   Influence of pyrocarbon amount in C/C preform on the microstructure and properties of C/ZrC composites prepared via reactive melt infiltration [J].
Chen, Si'an ;
Zhang, Changrui ;
Zhang, Yudi ;
Hu, Haifeng .
MATERIALS & DESIGN, 2014, 58 :570-576
[4]   Influence of SPS parameters on the density and mechanical properties of sintered Ti3SiC2 powders [J].
El Saeed, M. A. ;
Deorsola, F. A. ;
Rashad, R. M. .
INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS, 2013, 41 :48-53
[5]   Processing, microstructure and ablation behavior of C/SiC-Ti3SiC2 composites fabricated by liquid silicon infiltration [J].
Fan, Xiaomeng ;
Yin, Xiaowei ;
Wang, Lei ;
Cheng, Laifei ;
Zhang, Litong .
CORROSION SCIENCE, 2013, 74 :98-105
[6]   Tough salami-inspired Cf/ZrB2 UHTCMCs produced by electrophoretic deposition [J].
Galizia, Pietro ;
Failla, Simone ;
Zoli, Luca ;
Sciti, Diletta .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2018, 38 (02) :403-409
[7]   Novel Cr2AlC MAX-phase/SiC fiber composites: Synthesis, processing and tribological response [J].
Gonzalez-Julian, J. ;
Llorente, J. ;
Bram, M. ;
Belmonte, M. ;
Guillon, O. .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2017, 37 (02) :467-475
[8]  
Heidenreich B., 2008, CERAMIC MATRIX COMPO, P113, DOI [DOI 10.1002/9783527622412, 10.1002/9783527622412.ch5, DOI 10.1002/9783527622412.CH5]
[9]  
Ho-Duc L. H., 2003, J ALLOY COMPD, V350, p35J
[10]   Synthesis and characterization of 0.3 Vf TiC-Ti3SiC2 and 0.3 Vf SiC-Ti3SiC2 composites [J].
Ho-Duc, LH ;
El-Raghy, T ;
Barsoum, MW .
JOURNAL OF ALLOYS AND COMPOUNDS, 2003, 350 (1-2) :303-312