Synthesis and characterization of hausmannite (Mn3O4) nanostructures

被引：73
作者：
Rani, B. Jansi [1 ]
Ravina, M. [1 ]
Ravi, G. [1 ]
Ravichandran, S. [2 ]
Ganesh, V. [3 ]
Yuvakkumar, R. [1 ]
机构：
[1] Alagappa Univ, Dept Phys, Nanomat Lab, Karaikkudi 630003, Tamil Nadu, India
[2] CSIR, Cent Electrochem Res Inst, CECRI, Electro InorganicDiv, Karaikkudi 630003, Tamil Nadu, India
[3] CSIR, Cent Electrochem Res Inst, CECRI, Electrod & Electrocatalysis EEC Div, Karaikkudi 630003, Tamil Nadu, India
来源：
SURFACES AND INTERFACES | 2018年 / 11卷
关键词：
Chemical synthesis; Composite; Nanostructure; Powder processing; Scanning electron microscopy (SEM); ELECTROCHEMICAL PERFORMANCE; TEMPLATED SYNTHESIS; MAGNETIC-PROPERTIES; CHEMICAL-SYNTHESIS; CONTROLLED SIZE; ANODE MATERIALS; NANOPARTICLES; MICROSPHERES; NANOWIRES; FILMS;
D O I：
10.1016/j.surfin.2018.02.007
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Hausmannite (Mn3O4) plate like nano-grains, coin like nano-sphere and nano-petals structure were respectively prepared employing co-precipitation, sol- gel and hydrothermal route. The obtained product was characterized comprehensively. High specific capacitance value of 462.70 F/g at 10 mV/s was achieved using hydrothermal method. The magnetic behavior of product both in ZFC and FC modes employing VSM study confirmed the paramagnetic behavior turned as ferrimagnetic while changed the mode from ZFC to FC. The product synthesized by hydrothermal method possessed the good coercivity value of about 1965 Oe at 5 K. The preparation protocols have dominant influence on structural, morphological, optical, electrochemical and magnetic properties of nanostructured materials.
引用
收藏
页码：28 / 36
页数：9
相关论文
共 49 条
[1]   Sonochemical synthesis and chracterization of Mn3O4 nanoparticles [J].
Baykal, Abdulhadi ;
Kavas, Hueseyin ;
Durmus, Zehra ;
Demir, Mine ;
Kazan, Sinan ;
Topkaya, Ramazan ;
Toprak, Muhammet S. .
CENTRAL EUROPEAN JOURNAL OF CHEMISTRY, 2010, 8 (03) :633-638
[2]   Structure analysis of aluminium silicon manganese nitride precipitates formed in grain-oriented electrical steels [J].
Bernier, Nicolas ;
Xhoffer, Chris ;
Van De Putte, Toni ;
Galceran, Montserrat ;
Godet, Stephane .
MATERIALS CHARACTERIZATION, 2013, 86 :116-126
[3]   Controlled synthesis of Mn3O4 nanoparticles in ionic liquids [J].
Bussamara, Roberta ;
Melo, Wellington W. M. ;
Scholten, Jackson D. ;
Migowski, Pedro ;
Marin, Graciane ;
Zapata, Maximiliano J. M. ;
Machado, Giovanna ;
Teixeira, Sergio R. ;
Novak, Miguel A. ;
Dupont, Jairton .
DALTON TRANSACTIONS, 2013, 42 (40) :14473-14479
[4]   The change of the local environment of MnO incorporated in the lead-germanate glassy network [J].
Chelcea, R. ;
Rada, S. ;
Culea, E. ;
Coroiu, I. .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 2016, 433 :45-50
[5]   Influence of the synthesis method on the porosity, microstructure and electrical properties of La0.7Sr0.3MnO3 cathode materials [J].
da Conceicao, Leandro ;
Silva, Camila R. B. ;
Ribeiro, Nielson F. P. ;
Souza, Mariana M. V. M. .
MATERIALS CHARACTERIZATION, 2009, 60 (12) :1417-1423
[6]   La0.7Sr0.3MnO3 nanopowders: Synthesis of different powders structures and real magnetic properties of nanomanganites [J].
Danilenko, Igor ;
Konstantinova, Tetyana ;
Volkova, Galina ;
Glazunova, Valentina .
MATERIALS CHARACTERIZATION, 2013, 82 :140-145
[7]   A novel chemical synthesis and characterization of Mn3O4 thin films for supercapacitor application [J].
Dubal, D. P. ;
Dhawale, D. S. ;
Salunkhe, R. R. ;
Pawar, S. M. ;
Lokhande, C. D. .
APPLIED SURFACE SCIENCE, 2010, 256 (14) :4411-4416
[8]   All-solid-state flexible thin film supercapacitor based on Mn3O4 stacked nanosheets with gel electrolyte [J].
Dubal, Deepak P. ;
Holze, Rudolf .
ENERGY, 2013, 51 :407-412
[9]   X-ray micro-tomography investigation of the foaming process in the system of waste glass-silica mud-MnO2 [J].
Ducman, V. ;
Korat, L. ;
Legat, A. ;
Mirtic, B. .
MATERIALS CHARACTERIZATION, 2013, 86 :316-321
[10]   PEG-Assisted Synthesis of Mn3O4 Nanoparticles: A Structural and Magnetic Study [J].
Durmus, Zehra ;
Tomas, Merve ;
Baykal, Abdulhadi ;
Kavas, Huseyin ;
Toprak, Muhammed S. .
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2011, 41 (07) :768-773
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