One-pot self-catalyzed synthesis and properties of multiferroic BiFeO3 single-phase crystallites by sucrose-assisted combustion

被引：11
|
作者：
Li, Tie [1 ]
Shen, Jianfeng [1 ]
Li, Na [2 ]
Ye, Mingxin [1 ,2 ]
机构：
[1] Fudan Univ, Dept Mat Sci, Shanghai 200433, Peoples R China
[2] Fudan Univ, Ctr Special Mat & Technol, Shanghai 200433, Peoples R China
来源：
JOURNAL OF ALLOYS AND COMPOUNDS | 2013年 / 548卷
关键词：
Ceramics; Solid state reaction; Catalysis; Thermal analysis; MICROWAVE-HYDROTHERMAL SYNTHESIS; NANOSIZED BISMUTH FERRITE; THIN-FILMS; DIELECTRIC BEHAVIOR; PURE; CERAMICS; DECOMPOSITION; NANOPARTICLES; DEPENDENCE; PRECURSOR;
D O I：
10.1016/j.jallcom.2012.09.010
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A facile and effective self-catalyzed sucrose combustion was developed to synthesize single-phase BiFeO3 (BFO) that exhibited unusual ferromagnetic properties. Microscopy techniques were employed to examine morphologies and structures of the BFO. Reaction mechanism of the formation of the BFO was deduced by using thermo-gravimetric analysis and differential scanning calorimetry. Moreover, optical properties of the BFO were investigated by using UV-vis spectroscopy. Both magnetization hysteresis loops and zero field-cooling/field-cooling indicated that BFO had typical characteristics of spin-glass. X-ray photoelectron spectroscopy was used to expose the origin of the magnetism of the sample. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码：89 / 95
页数：7
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