Synthesis of azomethylene derivatives of 4-chloro-5H-1,2,3-dithiazole

被引：3

作者：

Yarovenko, VN

Es'kov, AA

Zatonsky, GV

Zavarzin, IV

Krayushkin, MM

Averkiev, BB

Antipin, MY

机构：

[1] Russian Acad Sci, ND Zelinskii Organ Chem Inst, Moscow 119991, Russia

[2] Russian Acad Sci, AN Nesmeyanov Organoelement Cpds Inst, Moscow 119991, Russia

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 2004年 / 41卷 / 01期

关键词：

D O I：

10.1002/jhet.5570410106

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Previously unknown azomethylene derivatives of 4-chloro-5H-1,2,3-dithiazole 5-7 were synthesized by the reaction of the Appel salt 1 with N-monosubstituted hydrazones 2-4. It was shown that they could be transformed into heterocyclic compounds 8-10.

引用

页码：37 / 43

页数：7

共 28 条

[1] 1,1′,2,2′,3,3′-tetrathiadiazafulvalenes;: preparation and characterisation of trans-[ClCNS2C=CS2NCCl] [J].

Barclay, TM ;

Cordes, AW ;

Oakley, RT ;

Preuss, KE ;

Reed, RW .

CHEMICAL COMMUNICATIONS, 1998, (09) :1039-1040

[2] Rapid synthesis of 2-cyanobenzothiazoles from N-aryliminodithiazoles under microwave irradiation [J].

Beneteau, V ;

Besson, T ;

Rees, CW .

SYNTHETIC COMMUNICATIONS, 1997, 27 (13) :2275-2280

[3] New route to 2-cyanobenzothiazoles via N-arylimino-1,2,3-dithiazoles [J].

Besson, T ;

Dozias, MJ ;

Guillard, J ;

Rees, CW .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1998, (23) :3925-3926

[4] Expeditious routes to 4-alkoxyquinazoline-2-carbonitriles and thiocarbamates via N-arylimino-1,2,3-dithiazoles using microwave irradiation [J].

Besson, T ;

Dozias, MJ ;

Guillard, J ;

Jacquault, P ;

Legoy, MD ;

Rees, CW .

TETRAHEDRON, 1998, 54 (23) :6475-6484

[5] Rapid synthesis of 2-cyanobenzothiazole, isothiocyanate and cyanoformanilide derivatives of dapsone [J].

Besson, T ;

Guillard, J ;

Rees, CW .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 2000, (04) :563-566

[6] Imidazoquinolinethiones from 8-aminoquinolines by a novel peri-participation [J].

Besson, T ;

Rees, CW ;

Roe, DG ;

Thiéry, V .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 2000, (04) :555-561

[7] New synthesis of isothiazoles from primary enamines [J].

Clarke, D ;

Emayan, K ;

Rees, CW .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1998, (01) :77-81

[8]

CLAUSSEN U, 1973, Patent No. 2210261

[9]

COX RA, 1975, CHEM HYDRAZO AZO A 2, P848

[10] Synthesis of novel dioxinobenzothiazole derivatives [J].

Guillard, J ;

Besson, T .

TETRAHEDRON, 1999, 55 (16) :5139-5144

← 1 2 3 →