Microstructural investigation of twin-roll cast magnesium AZ31B subjected to a single monotonic compressive stress

被引:5
作者
Whitmore, L. C. [1 ]
Denk, J. [2 ]
Zickler, G. A. [1 ]
Bourret, G. R. [1 ]
Huber, O. [2 ]
Saage, H. [2 ]
Huesing, N. [1 ]
Diwald, O. [1 ]
机构
[1] Paris Lodron Univ Salzburg, Chem & Phys Mat, A-5020 Salzburg, Austria
[2] Univ Appl Sci Landshut, Competence Ctr Lightweight Design, D-84036 Landshut, Germany
关键词
Precipitation; Magnesium-alloy; Transmission-electron-microscopy; Twinning; AZ31B; ALLOYS; DEFORMATION; SLIP; MG; PRECIPITATION; INDENTATION; STRENGTH; BEHAVIOR; TEXTURE; SIZE;
D O I
10.1016/j.jallcom.2019.03.068
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
In this research paper the microstructure of the magnesium AZ31B alloy is investigated after the application of a single monotonic compressive strain of -0.4%. A band of twinned grains is observed to form in the test bar approximately 10 mm wide, corresponding to the zone of highest plastic strain. The microstructure of this region is studied using electron backscatter diffraction and transmission electron microscopy (TEM). Twinning mode and fraction are reported along with a detailed analysis of precipitate phase and size distribution. Evidence is given for twin-precipitate interaction during the twin formation process. High resolution TEM and energy dispersive X-ray spectroscopy are used in conjunction with structural simulation software to identify the Al-Mn phase. A zinc shell is observed forming around precipitates, and this is related to zinc exclusion by the precipitating Al-Mn phase. (C) 2019 Elsevier B.V. All rights reserved.
引用
收藏
页码:1022 / 1034
页数:13
相关论文
共 64 条
[1]   Yield strength prediction in Ni-base alloy 718Plus based on thermo-kinetic precipitation simulation [J].
Ahmadi, M. R. ;
Povoden-Karadeniz, E. ;
Whitmore, L. ;
Stockinger, M. ;
Falahati, A. ;
Kozeschnik, E. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2014, 608 :114-122
[2]   SOLID SOLUTION STRENGTHENING OF MAGNESIUM SINGLE CRYSTALS .I. ALLOYING BEHAVIOUR IN BASAL SLIP [J].
AKHTAR, A ;
TEGHTSOONIAN, E .
ACTA METALLURGICA, 1969, 17 (11) :1339-+
[3]  
[Anonymous], 1957, JOM
[4]  
[Anonymous], PHYS METALLURGY MAGN
[5]  
[Anonymous], MAGNESIUM ALLOYS THE
[6]   Twinning and the ductility of magnesium alloys Part I: "Tension" twins [J].
Barnett, M. R. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2007, 464 (1-2) :1-7
[7]   Influence of grain size on the compressive deformation of wrought Mg-3Al-1Zn [J].
Barnett, MR ;
Keshavarz, Z ;
Beer, AG ;
Atwell, D .
ACTA MATERIALIA, 2004, 52 (17) :5093-5103
[8]  
Beausir B., 2015, ATOM - Analysis Tools for Orientation Maps
[9]  
Beausir B., 2017, Analysis tools for electron and X-ray diffraction, ATEX-software
[10]  
Bettles C, 2012, WOODHEAD PUBL MATER, pXIII