Near infrared spectroscopy as a tool for the rapid analysis of the Honeysuckle extracts

被引:25
作者
Li, Wenlong [1 ]
Wang, Yuefei [2 ]
Qu, Haibin [1 ]
机构
[1] Zhejiang Univ, Pharmaceut Informat Inst, Hangzhou 310058, Zhejiang, Peoples R China
[2] Tianjin Univ Tradit Chinese Med, State Key Lab Modern Chinese Med, Tianjin 300193, Peoples R China
关键词
Near infrared spectroscopy; Organic acids; Honeysuckle extract; Partial least squares regression; PERFORMANCE LIQUID-CHROMATOGRAPHY; JOHNS-WORT EXTRACTS; NIR SPECTROSCOPY; QUANTIFICATION;
D O I
10.1016/j.vibspec.2012.07.005
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
There is a lack of methods to analyze large numbers of traditional Chinese medicine (TCM) samples quickly and efficiently. Here we present a near infrared (NIR) spectroscopy-based method for the rapid analysis of Honeysuckle extracts. NIR spectra of 124 Honeysuckle extract samples produced within a four-year period were collected in the diffuse reflection mode and pretreated with multiplicative scatter correction (MSC). smoothing and derivative. Using partial least squares regression (PLSR), including PLS1 and PLS2, we established and validated the calibration models of six organic acids. Our results showed that both accuracy and precision of the NIR spectroscopy-based method meet the requirements of a traditional Chinese medicine (TCM) factory. This new method has the potential to save time, efforts and cost associated with the analysis of large quantities of unknown samples and will be particularly kapplicable to TCM factories for cost reduction. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:159 / 164
页数:6
相关论文
共 19 条
  • [1] [Anonymous], 2007, HDB NEAR INFRARED AN
  • [2] Brereton R.G., 2003, Chemometrics, P271
  • [3] Analysis of berberine and total alkaloid content in Cortex Phellodendri by near infrared spectroscopy (NIRS) compared with high-performance liquid chromatography coupled with ultra-visible spectrometric detection
    Chan, Chi-On
    Chu, Ching-Ching
    Mok, Daniel Kam-Wah
    Chau, Foo-Tim
    [J]. ANALYTICA CHIMICA ACTA, 2007, 592 (02) : 121 - 131
  • [4] Analysis of plant extracts by NIRS:: simultaneous determination of kavapyrones and water in dry extracts of Piper methysticum Forst.
    Gaub, M
    Roeseler, C
    Roos, G
    Kovar, KA
    [J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2004, 36 (04) : 859 - 864
  • [5] Comparative analysis of naphthodianthrone and phloroglucine derivatives in St. John's Wort extracts by near infrared spectroscopy, high-performance liquid chromatography and capillary electrophoresis
    Huck, C. W.
    Abel, G.
    Popp, M.
    Bonn, G. K.
    [J]. ANALYTICA CHIMICA ACTA, 2006, 580 (02) : 223 - 230
  • [6] Rapid analysis of Radix puerariae by near-infrared spectroscopy
    Lau, Ching-Ching
    Chan, Chi-On
    Chau, Foo-Tim
    Mok, Daniel Kam-Wah
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2009, 1216 (11) : 2130 - 2135
  • [7] [李文龙 LI Wen-long], 2009, [药物分析杂志, Chinese Journal of Pharmaceutical Analysis], V29, P1602
  • [8] Classification and quantification analysis of Radix scutellariae from different origins with near infrared diffuse reflection spectroscopy
    Li, Wenlong
    Xing, Lihong
    Cai, Yu
    Qu, Haibin
    [J]. VIBRATIONAL SPECTROSCOPY, 2011, 55 (01) : 58 - 64
  • [9] Application of near infrared spectroscopy for rapid analysis of intermediates of Tanreqing injection
    Li, Wenlong
    Xing, Lihong
    Fang, Limin
    Wang, Jue
    Qu, Haibin
    [J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2010, 53 (03) : 350 - 358
  • [10] Rapid quantification of phenolic acids in Radix Salvia Miltrorrhiza extract solutions by FT-NIR spectroscopy in transflective mode
    Li, Wenlong
    Qu, Haibin
    [J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2010, 52 (04) : 425 - 431