Programmed temperature vaporiser-based injection in capillary gas chromatography

被引:40
作者
Engewald, W
Teske, J
Efer, J
机构
[1] Univ Leipzig, Inst Analyt Chem, Fac Chem & Mineral, D-04103 Leipzig, Germany
[2] Univ Leipzig, Inst Legal Med, D-04103 Leipzig, Germany
关键词
reviews; programmed temperature vaporisers; large-volume injection; injection methods;
D O I
10.1016/S0021-9673(99)00723-2
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The application of programmed temperature vaporisation (PTV) in capillary I:as chromatographic analysis is reviewed. The development of the different strategies as well as the state of the art are described. As the analytes are normally enriched in the PTV insert, the quoted papers are subdivided depending on whether the enrichment was carried out from organic solvents, from water or from gaseous media. Furthermore, the possibilities of PTVs for on-line coupling with sample preparation methods or other separation techniques and their use as thermoreactors are mentioned. (C) 1999 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:259 / 278
页数:20
相关论文
共 115 条
  • [1] EVALUATION OF VENTED PROGRAMMED TEMPERATURE PRECOLUMNS IN GAS-LIQUID CHROMATOGRAPHY
    ABEL, K
    [J]. JOURNAL OF CHROMATOGRAPHY, 1964, 13 (01): : 14 - &
  • [2] Baltussen E, 1998, HRC-J HIGH RES CHROM, V21, P645
  • [3] Baltussen E, 1997, HRC-J HIGH RES CHROM, V20, P395, DOI 10.1002/jhrc.1240200710
  • [4] Baltussen E, 1997, HRC-J HIGH RES CHROM, V20, P385
  • [5] USE OF A PROGRAMMED-TEMPERATURE VAPORIZER FOR OFF-LINE SFE/GC ANALYSIS IN FOOD COMPOSITION STUDIES
    BLANCH, GP
    IBANEZ, E
    HERRAIZ, M
    REGLERO, G
    [J]. ANALYTICAL CHEMISTRY, 1994, 66 (06) : 888 - 892
  • [6] BLATT CR, 1991, HRC-J HIGH RES CHROM, V14, P775
  • [7] BODERIUS U, 1995, HRC-J HIGH RES CHROM, V18, P573
  • [8] Large-volume injection in capillary gas chromatography using a programmed-temperature vaporizing injector in the on-column or solvent-vent injection mode
    Bosboom, JC
    Janssen, HG
    Mol, HGJ
    Cramers, CA
    [J]. JOURNAL OF CHROMATOGRAPHY A, 1996, 724 (1-2) : 384 - 391
  • [9] BRAUNSTEIN L, 1990, VOM WASSER, V75, P1
  • [10] BREMER R, 1992, P 14 INT S CAP CHROM, P206