Investigation of temperature dependence of fracture toughness in high-dose HT9 steel using small-specimen reuse technique

The temperature dependence of fracture toughness in HT9 steel irradiated to 3-145 dpa at 380-503 degrees C was investigated using miniature three-point bend (TPB) fracture specimens. A miniature-specimen reuse technique has been established: the tested halves of subsize Charpy impact specimens with dimensions of 27 mm x 3 mm x 4 mm were reused for this fracture test campaign by cutting a notch with a diamond-saw in the middle of each half, and by fatigue-precracking to generate a sharp crack tip. It was confirmed that the fracture toughness of HT9 steel in the dose range depends more strongly on the irradiation temperature than the irradiation dose. At an irradiation temperature <430 degrees C, the fracture toughness of irradiated HT9 increased with the test temperature, reached an upper shelf of 180-200 MPa root m at 350-450 degrees C, and then decreased with the test temperature. At an irradiation temperature >= 430 degrees C, the fracture toughness was nearly unchanged up to about 450 degrees C and decreased slowly with test temperatures in a higher temperature range. Such a rather monotonic test temperature dependence after high-temperature irradiation is similar to that observed for an archive material generally showing a higher degree of toughness. A brittle fracture without stable crack growth occurred in only a few specimens with relatively lower irradiation and test temperatures. In this discussion, these TPB fracture toughness data are compared with previously published data from 12.7 mm diameter disc compact tension (DCT) specimens. (C) 2013 Elsevier B.V. All rights reserved.