Ethyl 6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

被引：5

作者：

Mohideen, M. Nizam ^{[1
]}

Pandi, A. Subbiah ^{[2
]}

Rasheeth, A. ^{[3
]}

Huq, C. A. M. A. ^{[3
]}

Nizar, S. Syed ^{[3
]}

机构：

[1] New Coll Autonomous, Dept Phys, Madras 600014, Tamil Nadu, India

[2] Presidency Coll Autonomous, Dept Phys, Madras 600005, Tamil Nadu, India

[3] New Coll Autonomous, Dept Chem, Madras 600014, Tamil Nadu, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536808025610

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C14H16N2O3, belongs to a group of esters of 2-oxo- and 1,2,3,4-tetrahydropyrimidine-5-carboxylic acids, which exhibit a wide spectrum of biological activities. The dihydropyrimidine ring adopts a screw-boat conformation. The crystal packing is stabilized by strong N - H center dot center dot center dot O and weak C - H center dot center dot center dot O intermolecular hydrogen bonds. An intramolecular C - H center dot center dot center dot O hydrogen bond is also present.

引用

页码：O1752 / U1888

页数：9

共 50 条

[41] Ethyl 4-(1,3-benzodioxol-5-yl)-6-methyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Nayak, Susanta K.
Venugopala, K. N.
Govender, Thavendran
Kruger, Hendrik G.
Maguire, Glenn E. M.
Row, Tayur N. Guru
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3069 - U1716
[42] Ethyl 1,6-dimethyl-2-oxo-4-(quinolin-4-yl)-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Zubatyuk, Roman I.
Shishkin, Oleg V.
Ihmels, Heiko
Lebedyeva, Iryna A.
Povstyanoy, Mykhaylo V.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1762 - U232
[43] Thermodynamic properties of methyl 4-(4-methoxyphenyl)-6-methl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate in organic solutions
Ridka, O.
Matiychuk, V
Sobechko, I
Tyshchenko, N.
Novyk, M.
Sergeev, V
Goshko, L.
FRENCH-UKRAINIAN JOURNAL OF CHEMISTRY, 2019, 7 (02): : 1 - 8
[44] Crystal structures of the anhydrous and two solvated forms of methyl 4-(4-fluorophenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Cleetus, Annie
Rani, Gulshan
Rao, G. B. Dharma
Chopra, Deepak
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2020, 76 : 786 - +
[45] Crystal structure of methyl 4-(2-fluorophenyl)-6-methyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Krishnamurthy, M. S.
Begum, Noor Shahina
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O838 - U387
[46] Synthesis, crystal structure and antibacterial properties of 6-methyl-2-oxo-4-(quinolin-2-yl)-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Huseynzada, A. E.
Jelsch, C.
Akhundzada, H. N.
Soudani, S.
Ben Nasr, C.
Doria, F.
Hasanova, U. A.
Freccero, M.
JOURNAL OF MOLECULAR STRUCTURE, 2020, 1219
[47] The dramatic effect of thiophenol on the reaction pathway of ethyl 4-chloromethyl-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate with thiophenolates: ring expansion versus nucleophilic substitution
Fesenko, Anastasia A.
Trafimova, Ludmila A.
Cheshkov, Dmitry A.
Shutalev, Anatoly D.
TETRAHEDRON LETTERS, 2010, 51 (38) : 5056 - 5059
[48] Ethyl 4-(2-fluorophenyl)-6-methyl-2-thioxo-1-(p-tolyl)-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Goncalves, Itamar Luis
Kagami, Luciano Porto
das Neves, Gustavo Machado
Rockenbach, Liliana
Davi, Leonardo
Soares, Alceu Felipe
Garcia, Solange Cristina
Eifler-Lima, Vera Lucia
MOLBANK, 2018, (04)
[49] Synthesis and characterization of ethyl-6-methyl-2-oxo-4-(3-(2,4,5-trifluorobenzamido)phenyl)-1,2,3,4-tetrahydropyrimidine-5-carboxylate. A DFT approach
Adaikalaraj, C.
Bhakiaraj, D.
Asha, Radhakrishnan Nandini
Sandosh, Thiruthuvadevaraj Antony
Manivarman, S.
Paularokiadoss, Francisxavier
VIETNAM JOURNAL OF CHEMISTRY, 2022, 60 (04) : 472 - 489
[50] Crystal structure of ethyl 4-(2-methoxy-phenyl)-6-methyl-2-sulfanylidene-1,2,3,4- tetrahydropyrimidine-5-carboxylate
Mohamed, Shaaban K.
Mague, Joel T.
Akkurt, Mehmet
Khodairy, Ahmed
Ahmed, Eman A.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O444 - U140

← 1 2 3 4 5 →