A low temperature synthesis of MnFe2O4 nanocrystals by microwave-assisted ball-milling

被引：66

作者：

Chen, Ding ^{[1
]}

Zhang, Yingzhe ^{[1
]}

Kang, Zhitao ^{[2
,3
]}

机构：

[1] Hunan Univ, Coll Mat Sci & Engn, Changsha 410082, Hunan, Peoples R China

[2] Georgia Inst Technol, Georgia Tech Res Inst, Atlanta, GA 30332 USA

[3] Georgia Inst Technol, Sch Mat Sci & Engn, Atlanta, GA 30332 USA

来源：

CHEMICAL ENGINEERING JOURNAL | 2013年 / 215卷

关键词：

MnFe2O4; Nanocrystals; Microwave-chemistry; Mechanochemistry; Ball milling; FERRITE; MN; NANOPARTICLES; SYSTEM;

D O I：

10.1016/j.cej.2012.10.061

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

In this paper, well-dispersed MnFe2O4 nanocrystals with high saturation magnetization were successfully prepared at a low temperature (below 100 degrees C) by a one step process through microwave-assisted ball milling in aqueous solution. The obtained nanocrystals were characterized by XRD, TEM, VSM. A lattice structure transition at a constant-temperature between tetragonal and cubic Mn3O4 intermediate product phases was observed during the reaction process. By the comparison of the as-milled products obtained with and without microwave-assistance, it was found that the coupling effect of ball-milling and microwave played a key role in the lattice transition and synthesis of MnFe2O4 nanocrystals. (C) 2012 Elsevier B.V. All rights reserved.

引用

页码：235 / 239

页数：5

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