2,4,6,8-Tetrakis(4-fluorophenyl)-3,7-diazabicyclo[3.3.1]nonan-9-one

被引：4

作者：

Natarajan, S. ^{[2
]}

Sudhapriya, V. ^{[3
]}

Vijayakumar, V. ^{[3
]}

Shoba, N. ^{[4
]}

Suresh, J. ^{[4
]}

Lakshman, P. L. Nilantha ^{[1
]}

机构：

[1] Univ Ruhuna, Dept Food Sci & Technol, Fac Agr, Mapalana 81100, Kamburupitiya, Sri Lanka

[2] Madurai Kamaraj Univ, Dept Phys, Madurai 625021, Tamil Nadu, India

[3] VIT Univ, Dept Chem, Vellore 632014, Tamil Nadu, India

[4] Madura Coll, Dept Phys, Madurai 625011, Tamil Nadu, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536808039135

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C31H24F4N2O, the bicyclo[3.3.1]nonane ring exists in a chair-boat conformation. Two of the four fluorine-substituted rings adopt equatorial dispositions with the piperidin-4-one rings. Molecules are linked into a two-dimensional network parallel to ((1) over bar 01) by N-H center dot center dot center dot O, C-H center dot center dot center dot F and C-H center dot center dot center dot O hydrogen bonds. Intermolecular N-H center dot center dot center dot pi and C-H center dot center dot center dot pi interactions are also observed.

引用

页码：O2496 / U3819

页数：12

共 7 条

[1]

Asakawa Y., 1995, PROGR CHEM ORGANIC N

[2]

Enraf-Nonius, 1994, CAD 4 EXPRESS

[3]

HARMS K, 1996, XCAD4

[4] CHEMISTRY OF 3-AZABICYCLO[3.3.1]NONANES [J].

JEYARAMAN, R ;

AVILA, S .

CHEMICAL REVIEWS, 1981, 81 (02) :149-174

[5] A SEMI-EMPIRICAL METHOD OF ABSORPTION CORRECTION [J].

NORTH, ACT ;

PHILLIPS, DC ;

MATHEWS, FS .

ACTA CRYSTALLOGRAPHICA SECTION A-CRYSTAL PHYSICS DIFFRACTION THEORETICAL AND GENERAL CRYSTALLOGRAPHY, 1968, A 24 :351-&

[6] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[7] Single-crystal structure validation with the program PLATON [J].

Spek, AL .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13

← 1 →