Synthesis of pd nanoparticles in La-doped mesoporous titania with polycrystalline framework

被引:17
作者
Yuan, S
Sheng, QR
Zhang, JL
Chen, F
Anpo, M
Dai, WL
机构
[1] E China Univ Sci & Technol, Adv Mat Lab, Shanghai 200237, Peoples R China
[2] E China Univ Sci & Technol, Inst Fine Chem, Shanghai 200237, Peoples R China
[3] Osaka Prefecture Univ, Grad Sch Engn, Dept Appl Chem, Sakai, Osaka 5998531, Japan
[4] Fudan Univ, Dept Chem, Shanghai 200433, Peoples R China
基金
中国国家自然科学基金;
关键词
Pd; photoreduction; mesoporous titania; polycrystalline framework;
D O I
10.1007/s10562-005-9726-x
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A simple synthetic method to prepare highly dispersed Pd nanoparticles in La-doped mesoporous titania with polycrystalline framework by coassembly and photoreduction is reported. The mesoporous materials were characterized by thermogravimetric (TGA)/differential scanning calorimetric (DSC), low angle and wide angle X-ray diffraction (XRD), transmission electron microscope (TEM), high-resolution transmission electron microscopy (HRTEM) and N(2) adsorption-desorption. The photocatalytic activities of the prepared mesoporous materials were evaluated by the photodegradation of methyl orange.
引用
收藏
页码:19 / 24
页数:6
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