Strain Localisation in iPP/MWCNT Nanocomposites Using Digital Image Correlation

Polypropylene/multiwall carbon nanotube nanocomposites with different rates of weight incorporation (0-1%) were prepared by melt compounding and cast extrusion. The effect of maleic anhydride (5wt%) grafted on polypropylene is studied through mechanical tests at different scales and morphological observations. In particular, the micromechanism of deformation was investigated through instrumented tensile experiments (at a macro and micro scales) using of a non-contact method known as digital image correlation. The objective of this paper is first to characterise global behaviour (Young modulus, tensile strength, and ultimate properties) and second to go further in local analysis. In particular, optical instrumentation enables estimation of strain profile distribution onto the sample in a constricted area. Statistical parameters extracted from these local profiles are promising tools to enhance mechanical properties in link with microstructural composition. Tensile tests confirm composite reinforcement at a low level of nanocomposite incorporation, and local analysis enables quantitative measurements of adding maleic anhydride in formulations. The results reveal that addition of maleic anhydride delays strain localisation in the necked area.