Characterization of Disinfection By-Products in Arkhangelsk Tap Water by Liquid Chromatography/High-Resolution Mass Spectrometry

被引：18
作者：
Kosyakov, D. S. [1 ]
Ul'yanovskii, N. V. [1 ]
Popov, M. S. [1 ]
Latkin, T. B. [1 ]
Lebedev, A. T. [1 ,2 ]
机构：
[1] Lomonosov Northern Arctic Fed Univ, Core Facil Ctr Arktika, Arkhangelsk 163002, Russia
[2] Moscow MV Lomonosov State Univ, Dept Chem, Moscow 119991, Russia
来源：
JOURNAL OF ANALYTICAL CHEMISTRY | 2018年 / 73卷 / 13期
基金：
俄罗斯科学基金会;
关键词：
high-resolution mass spectrometry; tandem mass spectrometry; chlorination; water disinfection; disinfection by-products; chlorophenols; MAMMALIAN-CELL CYTOTOXICITY; DISSOLVED ORGANIC-MATTER; DRINKING-WATER; EMERGING CONTAMINANTS; AQUATIC CHLORINATION; AVOBENZONE; DBPS;
D O I：
10.1134/S1061934818130099
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Disinfection of drinking water with chlorine-containing reagents leads to the formation of a large number of disinfection by-products, resulting from the chlorination of natural dissolved organic matter. High-performance liquid chromatography/high-resolution mass spectrometry with solid-phase preconcentration on a polymeric sorbent was used to study the component composition of halogen-containing disinfection by-products in Arkhangelsk tap water. Fourteen chlorinated and brominated organic compounds, which belong to the classes of halophenols, aromatic acids, carbonyl compounds, and chlorine-substituted nitrogen-containing heterocyclic compounds, have been found. Based on the analysis of MS/MS spectral data, possible structures of the detected disinfection by-products are proposed.
引用
收藏
页码：1260 / 1268
页数：9
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