Crystal structure of a new quasi-two-dimensional compound containing 1,4-bis(imidazol-1-ylmethyl)benzene (bix) and MnII ions

被引：35

作者：

Shen, HY

Liao, DZ ^{[1
]}

Jiang, ZH

Yan, SP

Wang, GL

Yao, XK

Wang, HG

机构：

[1] Nankai Univ, Dept Chem, Tianjin 300071, Peoples R China

[2] Nanjing Univ, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China

[3] Nankai Univ, Cent Lab, Tianjin 300071, Peoples R China

来源：

ACTA CHEMICA SCANDINAVICA | 1999年 / 53卷 / 06期

关键词：

D O I：

10.3891/acta.chem.scand.53-0387

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

A novel Mn-II complex Mn(bix)(3)(NO2)(2). 4H(2)O [bix = 1, 4-bis(imidazol-1-yl methyl)benzene] has been synthesized and characterized by X-ray single crystal structure analysis. The complex crystallizes in the P (1) over bar space group, with lattice parameters a = 9.037(2), b = 11.498(2), c = 12.404(2) Angstrom, alpha = 110.09(3), beta = 109.62(3), gamma = 93.05(3)degrees, V = 1119(1) Angstrom(3), D-c = 1.385 Mg m(-3), Z = 1, R-1 = 0.072, wR(2) = 0.0725. The X-ray analysis shows that it is a quasi-two-dimensional network containing hydrogen bonds, terminal and bridging bix ligands concurrently.

引用

页码：387 / 390

页数：4

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