Crystal structure of a new quasi-two-dimensional compound containing 1,4-bis(imidazol-1-ylmethyl)benzene (bix) and MnII ions

被引：35
作者：
Shen, HY
Liao, DZ [1 ]
Jiang, ZH
Yan, SP
Wang, GL
Yao, XK
Wang, HG
机构：
[1] Nankai Univ, Dept Chem, Tianjin 300071, Peoples R China
[2] Nanjing Univ, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China
[3] Nankai Univ, Cent Lab, Tianjin 300071, Peoples R China
来源：
ACTA CHEMICA SCANDINAVICA | 1999年 / 53卷 / 06期
关键词：
D O I：
10.3891/acta.chem.scand.53-0387
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
A novel Mn-II complex Mn(bix)(3)(NO2)(2). 4H(2)O [bix = 1, 4-bis(imidazol-1-yl methyl)benzene] has been synthesized and characterized by X-ray single crystal structure analysis. The complex crystallizes in the P (1) over bar space group, with lattice parameters a = 9.037(2), b = 11.498(2), c = 12.404(2) Angstrom, alpha = 110.09(3), beta = 109.62(3), gamma = 93.05(3)degrees, V = 1119(1) Angstrom(3), D-c = 1.385 Mg m(-3), Z = 1, R-1 = 0.072, wR(2) = 0.0725. The X-ray analysis shows that it is a quasi-two-dimensional network containing hydrogen bonds, terminal and bridging bix ligands concurrently.
引用
收藏
页码：387 / 390
页数：4
相关论文
共 50 条
[21]   Poly[[sesqui[μ2-1,4-bis(imidazol-1-ylmethyl)benzene-κ2N:N′](carbonato-κ2O,O′)copper(II)] 1,4-bis(imidazol-1-ylmethyl)benzene hemisolvate pentahydrate] [J].
Dai, Yu-Mei ;
Tang, En ;
Huang, Jin-Feng ;
Yang, Qiu-Yan .
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2008, 64 (10) :M349-M352
[22]   Synthesis, Crystal Structure, and Fluorescent Property of a New Two-Dimensional Zn(II) Coordination Polymer Based on Oxalic Acid and 1,4-Bis(imidazol-1-ylmethyl)-butane [J].
Li, Xiu-Mei ;
Qi, Xiao-Fei ;
Ji, Jian-Ye ;
Niu, Yan-Ling ;
Wang, Qing-Wei .
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2014, 44 (05) :765-770
[23]   Syntheses and structural characterization of iron(II) coordination polymers with flexible 1,4-bis(imidazol-1-ylmethyl) benzene ligand [J].
Beheshti, Azizolla ;
Lalegani, Arash ;
Bruno, Giuseppe ;
Rudbari, Hadi Amiri ;
Nobakht, Valiollah .
INORGANICA CHIMICA ACTA, 2013, 408 :214-221
[24]   Synthesis and Characterization of Two 2D Layered New Coordination Polymers of Co/Ni with the Ligand of 1,4-Bis(imidazol-1-ylmethyl)benzene [J].
Yang Xiao-Li ;
Zhang Jun ;
Li Yi-Zhi ;
Du Hong-Bin ;
You Xiao-Zeng .
CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2010, 26 (03) :374-378
[25]   A ratiometric fluorescence recognition of guanosine triphosphate on the basis of Zn(II) complex of 1,4-bis(imidazol-1-ylmethyl) benzene [J].
Liang, Li Jiao ;
Zhen, Shu Jun ;
Zhao, Xi Juan ;
Huang, Cheng Zhi .
ANALYST, 2012, 137 (22) :5291-5296
[26]   Hydrothermal Synthesis and Crystal Structure of Nickel(II) Coordination Polymer Assembled by 5-Nitroisophthalic Acid and 1,4-Bis(imidazol-1-ylmethyl)-benzene Ligands [J].
Li Xiu-Mei ;
Ji Jian-Ye ;
Niu Yan-Ling ;
Wang Zhi-Tao .
CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2013, 29 (01) :165-169
[27]   Poly[[μ2-1,4-bis(imidazol-1-ylmethyl)benzene]bis(μ4-cyclohexane-1,4-dicarboxylato)dicobalt(II)] [J].
Yu, Qun-Di ;
Sun, Da-Jun ;
Tiekink, Edward R. T. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :M1165-+
[28]   Syntheses, structures and photoluminescent properties of two zinc(II) coordination polymers based on aromatic polycarboxylate and 1,4-bis(imidazol-1-ylmethyl)benzene [J].
Liu, Guang-Xiang ;
Zhu, Kun ;
Nishihara, Sadafumi ;
Huang, Rong-Yi ;
Ren, Xiao-Ming .
INORGANICA CHIMICA ACTA, 2009, 362 (14) :5103-5108
[29]   Synthesis and Crystal Structure of a New Cadmium(II) Complex with 3,4-Pyridinedicarboxylic Acid and 1,4-Bis(imidazol-1-ylmethyl)-butane Ligands [J].
Liu Bo ;
Guo Jia ;
Zhou Shi ;
Wang Qing-Wei ;
Li Xiu-Mei ;
Li Chuan-Bi .
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2012, 31 (12) :1752-1756
[30]   Hydrothermal Synthesis and Crystal Structure of a Co(II) Coordination Polymer Assembled by 2,4-Pyridinedicarboxylic Acid and 1,4-Bis(imidazol-1-ylmethyl)-benzene) Ligands [J].
Li Xiu-Mei ;
Guo Jia ;
Wang Qing-Wei ;
Ji Jian-Ye ;
Wang Zhi-Tao .
CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2012, 28 (07) :1520-1524
12345