Novel Stationary Phases for Ion Chromatography and Hydrophilic Interaction Liquid Chromatography

被引:7
作者
Zatirakha, A. V. [1 ]
Uzhel, A. S. [1 ]
Loshin, A. A. [1 ]
Chernobrovkina, A. V. [1 ]
Smolenkov, A. D. [1 ]
Shpigun, O. A. [1 ]
机构
[1] Moscow MV Lomonosov State Univ, Dept Chem, Moscow 119991, Russia
关键词
ion chromatography; hydrophilic interaction liquid chromatography; adsorbent; anion exchanger; determination of anions; determination of polar compounds; ANION-EXCHANGERS; SILICA; SORBENTS; LAYERS;
D O I
10.1134/S106193481811014X
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
sThe review covers the research of the Laboratory of Chromatography of the Division of Analytical Chemistry of the Department of Chemistry of Moscow State University in the development of new stationary phases for hydrophilic interaction liquid chromatography and ion chromatography performed in 2007-2017. The principles that guided the team in selecting matrices for each type of adsorbents, approaches to the modification of surface, and the methods of forming functional layers are discussed. The revealed regularities of changes in the chromatographic properties of materials on varying the structural fragments of the functional layers are described in detail, which enabled the authors to develop approaches to obtaining stationary phases that are not inferior to commercial analogs in efficiency and selectivity.
引用
收藏
页码:12 / 20
页数:9
相关论文
共 24 条
[1]  
Chernobrovkina A. V., 2017, 45 INT S HIGH PERF L, P46
[2]   Mobile phases for the determination of polarizable anions on polystyrene/divinylbenzene anion-exchange resins [J].
Kas'yanova T.N. ;
Smolenkov A.D. ;
Pirogov A.V. ;
Shpigun O.A. .
Moscow University Chemistry Bulletin, 2007, 62 (5) :290-294
[3]   Synthesis of polymeric anion exchangers bearing dimethylhydrazine and alkylammonium functional groups and comparison of their chromatographic properties [J].
Kasiyanova, T. N. ;
Smolenkov, A. D. ;
Pirogov, A. V. ;
Shpigun, O. A. .
JOURNAL OF ANALYTICAL CHEMISTRY, 2008, 63 (01) :41-45
[4]  
Kasyanova T.N., 2007, SORBTS KHROMATOGR PR, V7, P52
[5]   MODIFIED SILICA AS A STATIONARY-PHASE FOR ION CHROMATOGRAPHY [J].
KROKHIN, OV ;
SMOLENKOV, AD ;
SVINTSOVA, NV ;
OBREZKOV, ON ;
SHPIGUN, OA .
JOURNAL OF CHROMATOGRAPHY A, 1995, 706 (1-2) :93-98
[6]  
[Кузнецова Ольга Игоревна Kuznetsova Olga I.], 2012, [Сорбционные и хроматографические процессы, Sorption and Chromatography Processes, Sorbtsionnye i khromatograficheskie protsessy], V12, P940
[7]   Chromatographic behavior of anions on polyelectrolyte sorbents based on silicagel [J].
Loshin A.A. ;
Zatirakha A.V. ;
Smolenkov A.D. ;
Shpigun O.A. .
Moscow University Chemistry Bulletin, 2015, 70 (1) :9-18
[8]   A novel covalently modified aminated silica-based anion exchanger for ion chromatography [J].
Loshin A.A. ;
Zatirakha A.V. ;
Smolenkov A.D. ;
Shpigun O.A. .
Moscow University Chemistry Bulletin, 2014, 69 (6) :245-253
[9]  
[Лошин А.А. Loshin A.A.], 2015, [Сорбционные и хроматографические процессы, Sorption and Chromatography Processes, Sorbtsionnye i khromatograficheskie protsessy], V15, P390
[10]   Silicas modified by polyelectrolyte complexes for the ion chromatography of anionic complexes of transition metals [J].
Pirogov, AV ;
Svintsova, NV ;
Kuzina, OV ;
Krokhin, OV ;
Platonov, MM ;
Shpigun, OA .
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1998, 361 (03) :288-293