An efficient synthesis of formylmethyl piperidine-1-carbodithioate diethyl acetal and analogs

被引:17
作者
Ge, ZM [1 ]
Li, RT [1 ]
Cheng, TM [1 ]
机构
[1] Beijing Med Univ, Sch Pharmaceut Sci, Beijing 100083, Peoples R China
关键词
D O I
10.1080/00397919908085943
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
The formylmethyl piperidine-1-carbodithioate diethyl acetal and its analogs were prepared from the reaction of different amines with carbon disulfide and bromoaldehyde acetal in the presence of anhydrous potassium phosphate under mild condition in excellent yield.
引用
收藏
页码:3191 / 3196
页数:6
相关论文
共 7 条
[1]   Synthesis of bromoacetals [J].
Bedoukian, PZ .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1944, 66 :651-652
[2]   RECENT PROGRESS ON CONDUCTING ORGANIC CHARGE-TRANSFER SALTS [J].
BRYCE, MR .
CHEMICAL SOCIETY REVIEWS, 1991, 20 (03) :355-390
[3]   THE REACTIVITY OF TETRATHIASELENAFULVALENES AND TETRASELENAFULVALENES [J].
GARIN, J .
ADVANCES IN HETEROCYCLIC CHEMISTRY, VOL 62, 1995, 62 :249-304
[4]   A simple one-pot preparation of dithiocarbamates in the presence of anhydrous potassium phosphate [J].
Li, RT ;
Ding, PY ;
Han, M ;
Cai, MS .
SYNTHETIC COMMUNICATIONS, 1998, 28 (02) :295-300
[5]  
Moore AJ, 1997, SYNTHESIS-STUTTGART, P407
[6]   BIS-1,3-DITHIOLIUM CHLORIDE - AN UNUSUALLY STABLE ORGANIC RADICAL CATION [J].
WUDL, F ;
SMITH, GM ;
HUFNAGEL, EJ .
JOURNAL OF THE CHEMICAL SOCIETY D-CHEMICAL COMMUNICATIONS, 1970, (21) :1453-&
[7]  
Zahradnik R., 1971, Int. J. Sulfur Chem. Part C, V6, P109