Solid phase analytical derivatization as a sample preparation method

被引：41

作者：

Atapattu, Sanka N. ^{[1
]}

Rosenfeld, Jack M. ^{[1
]}

机构：

[1] McMaster Univ, Dept Pathol & Mol Med, Hamilton, ON L8S 4K1, Canada

来源：

JOURNAL OF CHROMATOGRAPHY A | 2013年 / 1296卷

关键词：

Solid phase analytical derivatization; Analytical derivatization; Sample preparation; Extractive alkylation; Phase transfer catalyst; CHROMATOGRAPHY-MASS SPECTROMETRY; SINGLE-DROP MICROEXTRACTION; ON-FIBER DERIVATIZATION; IN-SITU DERIVATIZATION; LIQUID-LIQUID MICROEXTRACTION; BAR SORPTIVE EXTRACTION; VOLATILE FATTY-ACIDS; GAS-CHROMATOGRAPHY; GC-MS; SYRINGE DERIVATIZATION;

D O I：

10.1016/j.chroma.2013.03.020

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Analytical derivatization (AD) is an important procedure in analysis as it improves the sensitivity, selectivity and chromatographic separation. Solid phase analytical derivatization (SPAD) combines extraction and derivatization into a single step fulfilling many aspects of a good sample preparation technique, which includes low organic solvent consumption, economical, ease of automation with any chromatographic system and applicability in a wide range of complicated matrices. In this review we have focused on wide applications of SPAD when used in combination with different sample preparation methods, such as solid phase extraction, ion exchange resins, solid phase microextraction, in-tube, microfluidic devices, and hollow fiber extraction methods. (C) 2013 Elsevier B.V. All rights reserved.

引用

页码：204 / 213

页数：10

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