Grain boundary diffusion of Dy films prepared by magnetron sputtering for sintered Nd-Fe-B magnets

被引:31
作者
Chen, W. [1 ]
Luo, J. M. [1 ]
Guan, Y. W. [1 ]
Huang, Y. L. [1 ]
Chen, M. [2 ]
Hou, Y. H. [1 ]
机构
[1] Nanchang Hangkong Univ, Sch Mat Sci & Engn, Nanchang 330063, Jiangxi, Peoples R China
[2] Harvard Univ, Harvard Med Sch, Boston, MA 02138 USA
基金
中国国家自然科学基金;
关键词
magnetron sputtering; Dy films; coercivity; RE-rich phases; RICH PHASE; ELECTROPHORETIC DEPOSITION; COERCIVITY ENHANCEMENT; PERMANENT-MAGNETS; NDFEB MAGNETS; TEMPERATURE; DEPENDENCE; MECHANISM;
D O I
10.1088/1361-6463/aab912
中图分类号
O59 [应用物理学];
学科分类号
摘要
Dy films, deposited on the surface of sintered Nd-Fe-B magnets by magnetron sputtering, were employed for grain boundary diffusion source. High coercivity sintered Nd-Fe-B magnets were successfully prepared. Effects of sputtering power and grain boundary diffusion processes (GBDP) on the microstructure and magnetic properties were investigated in detail. The dense and uniform Dy films were beneficial to prepare high coercivity magnets by GBDP. The maximum coercivity value of 1189 kA m(-1) could be shown, which was an amplification of 22.3%, compared with that of as-prepared Nd-Fe-B magnet. Furthermore, the improved remanence and maximum energy product were also achieved through tuning grain boundary diffusion processes. Our results demonstrated that the formation of (Nd, Dy)(2)Fe14B shell surrounding Nd2Fe14B grains and fine, uniform and continuous intergranular RE-rich phases jointly contribute to the improved coercivity.
引用
收藏
页数:8
相关论文
共 25 条
[1]   Effect of rare earth content on TbF3 diffusion in sintered Nd-Fe-B magnets by electrophoretic deposition [J].
Cao, Xuejing ;
Chen, Ling ;
Guo, Shuai ;
Fan, Fengchun ;
Chen, Renjie ;
Yan, Aru .
SCRIPTA MATERIALIA, 2017, 131 :24-28
[2]   Nanophase hard magnets [J].
Hadjipanayis, GC .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 1999, 200 (1-3) :373-391
[3]   EFFECTS OF CO ADDITION ON THE TEMPERATURE-DEPENDENCE OF THE INTRINSIC-COERCIVITY IN PR-FE-B SINTERED MAGNETS [J].
HIROSAWA, S ;
SAGAWA, M .
JOURNAL OF APPLIED PHYSICS, 1988, 64 (10) :5553-5555
[4]   Coercivity enhancement by the grain boundary diffusion process to Nd-Fe-B sintered magnets [J].
Hirota, K. ;
Nakamura, H. ;
Minowa, T. ;
Honshima, M. .
IEEE TRANSACTIONS ON MAGNETICS, 2006, 42 (10) :2909-2911
[5]   Strategy for high-coercivity Nd-Fe-B magnets [J].
Hono, K. ;
Sepehri-Amin, H. .
SCRIPTA MATERIALIA, 2012, 67 (06) :530-535
[6]   Effects of Nd-rich phase on the improved properties and recoil loops for hot deformed Nd-Fe-B magnets [J].
Hou, Y. H. ;
Wang, Y. L. ;
Huang, Y. L. ;
Wang, Y. ;
Li, S. ;
Ma, S. C. ;
Liu, Z. W. ;
Zeng, D. C. ;
Zhao, L. Z. ;
Zhong, Z. C. .
ACTA MATERIALIA, 2016, 115 :385-391
[7]   Influence of annealing temperature on the Dy diffusion process in NdFeB magnets [J].
Hu, Sheng-Qing ;
Peng, Kun ;
Chen, Hong .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2017, 426 :340-346
[8]   Magnetic microstructure and magnetic properties of spark plasma sintered NdFeB magnets [J].
Huang, Y. L. ;
Wang, Y. ;
Hou, Y. H. ;
Wang, Y. L. ;
Wu, Y. ;
Ma, S. C. ;
Liu, Z. W. ;
Zeng, D. C. ;
Tian, Y. ;
Xia, W. X. ;
Zhong, Z. C. .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2016, 399 :175-178
[9]   Anisotropic diffusion mechanism in grain boundary diffusion processed Nd-Fe-B sintered magnet [J].
Kim, Tae-Hoon ;
Lee, Seong-Rae ;
Yun, Seok Jin ;
Lim, Sang Ho ;
Kim, Hyo-Jun ;
Lee, Min-Woo ;
Jang, Tae-Suk .
ACTA MATERIALIA, 2016, 112 :59-66
[10]   Simultaneous application of Dy-X (X = F or H) powder doping and dip-coating processes to Nd-Fe-B sintered magnets [J].
Kim, Tae-Hoon ;
Lee, Seong-Rae ;
Kim, Hyo-Jun ;
Lee, Min-Woo ;
Jang, Tae-Suk .
ACTA MATERIALIA, 2015, 93 :95-104