An efficient and novel method for the synthesis of sulfinate esters under solvent-free conditions

被引：42

作者：

Hajipour, AR ^{[1
]}

Falahati, AR

Ruoho, AE

机构：

[1] Isfahan Univ Technol, Dept Chem, Pharmaceut Res Lab, Esfahan 84156, Iran

[2] Univ Wisconsin, Sch Med, Dept Pharmacol, Madison, WI 53706 USA

来源：

TETRAHEDRON LETTERS | 2006年 / 47卷 / 16期

基金：

美国国家卫生研究院;

关键词：

DCC; solvent-free; sulfinic acids; sulfinate esters;

D O I：

10.1016/j.tetlet.2006.02.080

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The present letter describes a reliable one-stage process for the preparation of sulfinate esters from the corresponding sulfinic acid and alcohols in the presence of N,N'-dicyclohexylcarbodiimide (DCC) under solvent-free conditions. (c) 2006 Elsevier Ltd. All rights reserved.

引用

页码：2717 / 2719

页数：3

共 46 条

[21]

Hajipour AR, 2000, SYNLETT, P740

[22] Iodination of aromatic compounds under mild and solvent-free conditions [J].

Hajipour, AR ;

Ruoho, AE .

ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 2002, 34 (06) :647-651

[23] Wet silica-supported permanganate for the cleavage of semicarbazones and phenylhydrazones under solvent-free conditions [J].

Hajipour, AR ;

Adibi, H ;

Ruoho, AE .

JOURNAL OF ORGANIC CHEMISTRY, 2003, 68 (11) :4553-4555

[24]

Hajipour AR, 2002, J CHEM RES, P547

[25] Tetramethylammonium dichloroiodate: An efficient and environmentally friendly iodination reagent for iodination of aromatic compounds under mild and solvent-free conditions [J].

Hajipour, AR ;

Arbabian, M ;

Ruoho, AE .

JOURNAL OF ORGANIC CHEMISTRY, 2002, 67 (24) :8622-8624

[26] Asymmetric reduction of prochiral cyclic imines to alkaloid derivatives by novel asymmetric reducing reagent in THF or under solid-state conditions [J].

Hajipour, AR ;

Hantehzadeh, M .

JOURNAL OF ORGANIC CHEMISTRY, 1999, 64 (23) :8475-8478

[27] Solid-phase synthesis of oximes [J].

Hajipour, AR ;

Mohammadpoor-Baltork, I ;

Nikbaghat, K ;

Imanzadeh, G .

SYNTHETIC COMMUNICATIONS, 1999, 29 (10) :1697-1701

[28]

Hajipour AR, 1999, CHEM LETT, P99

[29] A rapid and convenient synthesis of oximes in dry media under microwave irradiation [J].

Hajipour, AR ;

Mallakpour, SE ;

Imanzadeh, G .

JOURNAL OF CHEMICAL RESEARCH, 1999, (03) :228-229

[30] Benzyltriphenylphosphonium peroxymonosulfate: As a novel and efficient reagent for oxidation of alcohols under solvent-free conditions [J].

Hajipour, AR ;

Mallakpour, SE ;

Adibi, H .

CHEMISTRY LETTERS, 2000, (05) :460-461

← 1 2 3 4 5 →