Assessment of lower-voltage TEM performance using 3D Fourier transform of through-focus series

被引:13
作者
Kimoto, Koji [1 ,3 ]
Kurashima, Keiji [1 ]
Nagai, Takuro [1 ]
Ohwada, Megumi [1 ]
Ishizuka, Kazuo [1 ,2 ]
机构
[1] Natl Inst Mat Sci, Tsukuba, Ibaraki 3050044, Japan
[2] HREM Res Inc, Higashimatsuyama, Saitama 3550055, Japan
[3] Japan Sci & Technol Agcy, Res Accelerat Program, Tokyo, Japan
关键词
High-resolution transmission electron microscopy; Low acceleration voltage; Spherical aberration corrector; Information limit; Young fringe; Monochromator; WAVE-FUNCTION RECONSTRUCTION; ENERGY-LOSS SPECTROSCOPY; HIGH-RESOLUTION; ABERRATION; HRTEM;
D O I
10.1016/j.ultramic.2012.06.012
中图分类号
TH742 [显微镜];
学科分类号
摘要
We assess the imaging performance of a transmission electron microscopy (TEM) system operated at a relatively low acceleration voltage using the three-dimensional (3D) Fourier transform of through-focus images. Although a single diffractogram and the Thon diagram cannot distinguish between the linear and non-linear TEM imaging terms, the 3D Fourier transform allows us to evaluate linear imaging terms, resulting in a conclusive assessment of TEM performance. Using this method, information transfer up to 98 pm is demonstrated for an 80 kV TEM system equipped with a spherical aberration corrector and a monochromator. We also revisit the Young fringe method in the light of the 3D Fourier transform, and have found a considerable amount of non-linear terms in Young fringes at 80 kV even from a typical standard specimen, such as an amorphous Ge thin film. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:31 / 37
页数:7
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