An efficient scalable synthesis of 2,3-epoxypropyl phenylhydrazones

被引：9

作者：

Getautis, V ^{[1
]}

Daskeviciene, M ^{[1
]}

Malinauskas, T ^{[1
]}

Stanisauskaite, A ^{[1
]}

Stumbraite, J ^{[1
]}

机构：

[1] Kaunas Univ Technol, Dept Organ Chem, LT-50270 Kaunas, Lithuania

来源：

MOLECULES | 2006年 / 11卷 / 01期

关键词：

heterocycles; epichlorohydrin; hydrazones; charge transport;

D O I：

10.3390/11010064

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

A series of mono and di-N-2,3-epoxypropyl N-phenylhydrazones have been prepared on a large scale by reaction of the corresponding N-phenylhydrazones of 9-ethyl-3-carbazolecarbaldehyde, 9-ethyl-3,6-carbazoledicarbaldehyde, 4-dimethylamino-, 4-diethylamino-, 4-benzylethylamino-, 4-(diphenylamino)-, 4-(4,4'-dimethyldiphenylamino)-, 4-(4-fortnyldiphenylamino)- and 4-(4-formyldiphenlamino-4'-methyldiphenylamino)benzaldehyde with epichlorohydrin in the presence of KOH and anhydrous Na2SO4.

引用

页码：64 / 71

页数：8

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