An efficient scalable synthesis of 2,3-epoxypropyl phenylhydrazones

被引：9
|
作者：
Getautis, V [1 ]
Daskeviciene, M [1 ]
Malinauskas, T [1 ]
Stanisauskaite, A [1 ]
Stumbraite, J [1 ]
机构：
[1] Kaunas Univ Technol, Dept Organ Chem, LT-50270 Kaunas, Lithuania
来源：
MOLECULES | 2006年 / 11卷 / 01期
关键词：
heterocycles; epichlorohydrin; hydrazones; charge transport;
D O I：
10.3390/11010064
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
A series of mono and di-N-2,3-epoxypropyl N-phenylhydrazones have been prepared on a large scale by reaction of the corresponding N-phenylhydrazones of 9-ethyl-3-carbazolecarbaldehyde, 9-ethyl-3,6-carbazoledicarbaldehyde, 4-dimethylamino-, 4-diethylamino-, 4-benzylethylamino-, 4-(diphenylamino)-, 4-(4,4'-dimethyldiphenylamino)-, 4-(4-fortnyldiphenylamino)- and 4-(4-formyldiphenlamino-4'-methyldiphenylamino)benzaldehyde with epichlorohydrin in the presence of KOH and anhydrous Na2SO4.
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页码：64 / 71
页数：8
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