[N-(5-Bromo-2-oxidobenzylidene)-L-valinato-κ3O,N,O′]diethyltin(IV)

被引:2
作者
Wang, Wei [1 ]
Tian, Laijin [1 ,2 ]
Chen, Dengtai [1 ]
Qu, Yuan [1 ]
机构
[1] Qufu Normal Univ, Dept Chem, Qufu 273165, Peoples R China
[2] Shandong Univ, Dept Chem, Jinan 250100, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷
关键词
D O I
10.1107/S1600536808032388
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The Sn atom of the title compound, [Sn(C2H5)(2)(C12H12BrNO3)], is in a distorted SnNC2O2 trigonal-bipyramidal geometry and forms five-and six-membered chelate rings with the tridentate ligand. One C atom of one ethyl group is disordered with site occupancies of 0.61 (3): 0.39 (3).
引用
收藏
页码:M1404 / U518
页数:10
相关论文
共 11 条
[1]   Self-assembly of extended Schiff base amino acetate skeletons, 2-{[(2Z)-(3-hydroxy-1-methyl-2-butenylidene)]amino} phenylpropionate and 2-{[(E)-1-(2-hydroxyaryl)alkylidene]amino} phenylpropionate skeletons incorporating organotin(IV) moieties:: Synthesis, spectroscopic characterization crystal structures, and in vitro cytotoxic activity [J].
Baul, Tushar S. Basu ;
Masharing, Cheerfulman ;
Ruisi, Giuseppe ;
Jirasko, Robert ;
Holcapek, Michal ;
de Vos, Dick ;
Wolstenholme, David ;
Linden, Anthony .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2007, 692 (22) :4849-4862
[2]   One-step preparation, structural assignment, and X-ray study of 2,2-di-n-butyl- and 2,2-diphenyl-6-aza-1,3-dioxa-2-stannabenzocyclononen-4-ones derived from amino acids [J].
Beltrán, HI ;
Zamudio-Rivera, LS ;
Mancilla, T ;
Santillan, R ;
Farfán, N .
CHEMISTRY-A EUROPEAN JOURNAL, 2003, 9 (10) :2291-2306
[3]  
*BRUK AXS INC, 2002, SADABS SAINT SMART
[4]   Synthesis, characterization, and X-ray structures of diphenyltin(IV) N-(2-hydroxyacetophenone)glycinate, its 1:1 adduct with triphenyltin(IV) chloride, and related systems [J].
Dakternieks, D ;
Baul, TSB ;
Dutta, S ;
Tiekink, ERT .
ORGANOMETALLICS, 1998, 17 (14) :3058-3062
[5]  
Farrugia L.J., 1997, J APPL CRYSTALLOGR, V30, P565
[6]   ON ENANTIOMORPH-POLARITY ESTIMATION [J].
FLACK, HD .
ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV) :876-881
[7]   Second-harmonic generation within the P212121 space group, in a series of chiral (salicylaldiminato)tin Schiff base complexes [J].
Rivera, JM ;
Reyes, H ;
Cortés, A ;
Santillan, R ;
Lacroix, PG ;
Lepetit, C ;
Nakatani, K ;
Farfán, N .
CHEMISTRY OF MATERIALS, 2006, 18 (05) :1174-1183
[8]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[9]   Synthesis, characterization and biological activity of diorganotin(IV) complexes of N-(3,5-dibromo-salicylidene)-α-amino acid [J].
Tian Lai-Jin ;
Sun Yu-Xi ;
Zheng Xiao-Liang ;
Liu Xi-Jie ;
Yu You ;
Liu Xue-Li ;
Qian Bo-Chu .
CHINESE JOURNAL OF CHEMISTRY, 2007, 25 (03) :312-318
[10]  
Tian LJ, 2006, APPL ORGANOMET CHEM, V20, P74, DOI 10.1002/aoc.1005