9-(2-chlorophenyl)-1,2,3,4,5,6,7,8,9,10-decahydro-3,3,6,6-tetramethylacridine-1,8-dione

被引：0

作者：

Rong, Liang-Ce ^{[1
]}

Li, Xiao-Yue ^{[1
]}

Yao, Chang-Sheng ^{[1
]}

Wang, Hai-Ying ^{[1
]}

Shi, Da-Qing ^{[1
]}

机构：

[1] Xuzhou Normal Univ, Dept Chem, Xuzhou 221116, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷

关键词：

D O I：

10.1107/S1600536806017788

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C23H26ClNO2, was synthesized by the reaction of 5,5-dimethyl-cyclo-hexane-1,3-dione with 4-chloro-N-(2-chloro-benzyl-idene)benzenamine under solvent-free conditions using triethylbenzylammonium chloride as catalyst at 353 K. The dihydro-pyridine ring of the mol-ecule adopts a half-chair conformation.

引用

页码：O2380 / O2381

页数：2

共 13 条

[1] ANNUNZIATA S, 1997, TETRAHEDRON LETT, V38, P289
[2] 4-ARYLDIHYDROPYRIDINES, A NEW CLASS OF HIGHLY-ACTIVE CALCIUM-ANTAGONISTS
BOSSERT, F
MEYER, H
WEHINGER, E
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1981, 20 (09): : 762 - 769
[3] BRUKER, 1999, SAINT VERSION 5 1 SH
[4] BRUKER, 1998, SMART VERSION 5 0
[5] New 1,4-dihydropyridines conjugated to furoxanyl moieties, endowed with both nitric oxide-like and calcium channel antagonist vasodilator activities
Di Stilo, A
Visentin, S
Cena, C
Gasco, AM
Ermondi, G
Gasco, A
[J]. JOURNAL OF MEDICINAL CHEMISTRY, 1998, 41 (27) : 5393 - 5401
[6] INTRAMOLECULAR MICHAEL-TYPE ADDITION IN THE SOLID-STATE
GOUD, BS
PANNEERSELVAM, K
ZACHARIAS, DE
DESIRAJU, GR
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1995, (02): : 325 - 330
[7] Solvent-free Knoevenagel condensations and Michael additions in the solid state and in the melt with quantitative yield
Kaupp, G
Naimi-Jamal, MR
Schmeyers, J
[J]. TETRAHEDRON, 2003, 59 (21) : 3753 - 3760
[8] 1-BENZYLDIHYDRONICOTINAMIDE - A MODEL FOR REDUCED DPN
MAUZERALL, D
WESTHEIMER, FH
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1955, 77 (08) : 2261 - 2264
[9] Syntheses, calcium channel agonist-antagonist modulation activities, and nitric oxide release studies of nitrooxyalkyl 1,4-dihydro-2,6-dimethyl-3-nitro-4-(2,1,3-benzoxadiazol-4-yl)pyridine-5-carboxylate racemates, enantiomers, and diastereomers
Shan, RD
Velazquez, C
Knaus, EE
[J]. JOURNAL OF MEDICINAL CHEMISTRY, 2004, 47 (01) : 254 - 261
[10] Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR

← 1 2 →