Optical properties of the mechanochemically synthesized Cu2FeSnS4 (stannite) nanocrystals: Raman study

被引：8
作者：
Trajic, J. [1 ]
Romcevic, M. [1 ]
Petrovic, M. [1 ]
Gilic, M. [1 ]
Balaz, P. [2 ]
Zorkovska, A. [2 ]
Romcevic, N. [1 ]
机构：
[1] Univ Belgrade, Inst Phys, Belgrade 11080, Serbia
[2] Slovak Acad Sci, Inst Geotech, Kosice 04353, Slovakia
来源：
OPTICAL MATERIALS | 2018年 / 75卷
关键词：
Nanostructures; Optical properties; X-ray diffraction; Raman spectroscopy; CU2ZNSNS4; THIN-FILMS; NANOPARTICLES; SULFURIZATION; SPECTROSCOPY; PRECURSORS; DEPOSITION; KESTERITE; SNS;
D O I：
10.1016/j.optmat.2017.10.043
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
The analysis of the vibrational properties of mechanochemically synthesized stannite Cu2FeSnS4 nano crystals has been performed. X-ray diffraction (XRD) and Raman spectroscopy are techniques used to characterize the crystal structure and compositional purity of stannite Cu2FeSnS4 nanoparticles. The detailed analysis of the experimental spectra has allowed us to determine the frequency and symmetry assignment of the main and weaker peaks. The milling time influence on synthesis stannite Cu2FeSnS4 from elemental precursors Cu, Fe, Sn and S is observed. Among the peaks that are characteristic for the stannite Cu2FeSnS4, we registered the modes of binary phases of FeS and SnS. The total disappearance of the binary phases of FeS and SnS is observed when the milling time is longer than 90 min. (C) 2017 Elsevier B.V. All rights reserved.
引用
收藏
页码：314 / 318
页数：5
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