Synthesis of 6-thioxo-1,2,5-oxadiazinan-3-ones and transformation into 3-amino-2-thiohydantoins and 3-hydroxy-2-thiohydantoins

被引：0

作者：

Geffken, D ^{[1
]}

Ploetz, A ^{[1
]}

机构：

[1] Univ Hamburg, Abt Pharmaceut Chem, Inst Pharm, D-20146 Hamburg, Germany

来源：

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 2006年 / 61卷 / 01期

关键词：

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

6-Thioxo-1,2,5-oxadiazinan-3-ones 5, easily available by cyclic thiocarbonylation of N",N-disubstituted alpha-aminocarbohydroxamic acids 4 with 1,1'-thiocarbonyldiimidazole, are transformed by hydrazine or hydroxylamine into 3-amino-2-thiohydantoins 6 and 3-hydroxy-2-thiohydantoins 7.

引用

页码：83 / 86

页数：4

共 50 条

[41] DEGRADATIVE STUDIES ON PEPTIDES AND PROTEINS .3. SYNTHESIS OF SOME 2-THIOHYDANTOINS AS REFERENCE COMPOUNDS
ELMORE, DT
OGLE, JR
TOSELAND, PA
JOURNAL OF THE CHEMICAL SOCIETY, 1956, (JAN): : 192 - 196
[42] COORDINATION-COMPOUNDS OF 6-THIOXO-1,2,3,6-TETRAHYDRO-1,2,4-TRIAZINE-5-THIOLATES
KIBBEL, HU
DANNENBERGER, D
KALIES, W
ZEITSCHRIFT FUR CHEMIE, 1989, 29 (09): : 336 - 336
[43] Synthesis 5-(pyrazolin-3-ylmethylidene)-2-thiohydantoins and 2-alkylsulfanyl-5-(pyrazolin-3-ylmethylidene)-3,5-dihydro-4H-imidazol-4-ones
Vorozhtsov, N. I.
Sviridova, L. A.
Grigorkevich, O. S.
Korablina, D. D.
Beloglazkina, E. K.
Majouga, A. G.
Zyk, N. V.
RUSSIAN CHEMICAL BULLETIN, 2017, 66 (03) : 506 - 510
[44] PSEUDOESTERS AND DERIVATIVES .6. SYNTHESIS OF 5-HYDROXY-3-PYRROLIN-2-ONES AND 5-METHOXY-3-PYRROLIN-2-ONES
FARINA, F
MARTIN, MV
PAREDES, MC
SYNTHESIS-STUTTGART, 1973, (03): : 167 - 168
[45] Synthesis 5-(pyrazolin-3-ylmethylidene)-2-thiohydantoins and 2-alkylsulfanyl-5-(pyrazolin-3-ylmethylidene)-3,5-dihydro-4H-imidazol-4-ones
N. I. Vorozhtsov
L. A. Sviridova
O. S. Grigorkevich
D. D. Korablina
E. K. Beloglazkina
A. G. Majouga
N. V. Zyk
Russian Chemical Bulletin, 2017, 66 : 506 - 510
[46] Synthesis of 2-aroylmethylidene-6-hydroxy-2,3-dihydroindol-3-ones
V. L. Gein
A. V. Demeneva
N. A. Rassudikhina
M. I. Vakhrin
Russian Journal of Organic Chemistry, 2006, 42 : 617 - 618
[47] Synthesis of 2-aroylmethylidene-6-hydroxy-2,3-dihydroindol-3-ones
Gein, V. L.
Demeneva, A. V.
Rassudikhina, N. A.
Vakhrin, M. I.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2006, 42 (04) : 617 - 618
[48] ELECTRON-IMPACT INDUCED FRAGMENTATION PATHWAYS OF THE 3-ALKYL-2-THIOHYDANTOINS
RYCZEK, J
CHEMIA ANALITYCZNA, 1994, 39 (06): : 719 - 727
[49] MICROCHEMICAL DETECTION OF COPPER BY COLOR-REACTION WITH SOME 3-PHENYL-2-THIOHYDANTOINS OF AMINO-ACIDS
GRUNER, K
CHEMICKE LISTY, 1973, 67 (11): : 1206 - 1207
[50] SYNTHESIS OF 3-BUTANOYL-4-HYDROXY-3-PYRROLIN-2-ONES AND 3-BENZOYL-4-HYDROXY-3-PYRROLIN-2-ONES AND THEIR COMPLEXES WITH METAL-IONS
MARKOPOULOU, O
MARKOPOULOS, J
NICHOLLS, D
JOURNAL OF INORGANIC BIOCHEMISTRY, 1990, 39 (04) : 307 - 316

← 1 2 3 4 5 →