Quantitative Analysis of Anatase-Rutile Mixtures by Raman Spectroscopy

被引:10
作者
Cao, Guoqiang [1 ]
Yi, Nan [1 ]
机构
[1] Univ New Hampshire, Dept Chem Engn, Durham, NH 03824 USA
基金
美国国家科学基金会;
关键词
Titanium dioxide; Anatase; Raman; PHASE-TRANSFORMATION; TIO2; KINETICS; SPECTRA;
D O I
10.1002/slct.202002931
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
We present how to calculate the weight fraction of anatase in the physical anatase-rutile mixture based on the analysis of Raman spectra. Raman-based correlation is also applicable to characterize quantitively the weight fraction of anatase from chemically synthesized anatase-rutile titanium dioxide mixtures.
引用
收藏
页码:11530 / 11533
页数:4
相关论文
共 25 条
[1]  
ALEXANDER L., 1948, Anal. Chem, V20, P886, DOI [DOI 10.1021/AC60022A002, 10.1021/ac60022a002]
[2]   RAMAN-SPECTRA OF TITANIUM-DIOXIDE [J].
BALACHANDRAN, U ;
EROR, NG .
JOURNAL OF SOLID STATE CHEMISTRY, 1982, 42 (03) :276-282
[3]  
Castrejón-Sánchez V.H., 2014, Superf. vacío, V27, P88
[4]   Influence of Brookite Impurities on the Raman Spectrum of TiO2 Anatase Nanocrystals [J].
Ceballos-Chuc, M. C. ;
Ramos-Castillo, C. M. ;
Alvarado-Gil, J. J. ;
Oskam, G. ;
Rodriguez-Gattorno, G. .
JOURNAL OF PHYSICAL CHEMISTRY C, 2018, 122 (34) :19921-19930
[5]   On-line analysis using Raman spectroscopy for process control during the manufacture of titanium dioxide [J].
Clegg, IM ;
Everall, NJ ;
King, B ;
Melvin, H ;
Norton, C .
APPLIED SPECTROSCOPY, 2001, 55 (09) :1138-1150
[6]   THE ANATASE-RUTILE TRANSITION .1. KINETICS OF THE TRANSFORMATION OF PURE ANATASE [J].
CZANDERNA, AW ;
RAO, CNR ;
HONIG, JM .
TRANSACTIONS OF THE FARADAY SOCIETY, 1958, 54 (07) :1069-1073
[7]   Raman spectra of titanium dioxide (anatase, rutile) with identified oxygen isotopes (16,17,18) [J].
Frank, Otakar ;
Zukalova, Marketa ;
Laskova, Barbora ;
Kuerti, Jenoe ;
Koltai, Janos ;
Kavan, Ladislav .
PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2012, 14 (42) :14567-14572
[8]   Kinetics of the anatase rutile transformation in TiO2 in the presence of Fe2O3 [J].
Gennari, FC ;
Pasquevich, DM .
JOURNAL OF MATERIALS SCIENCE, 1998, 33 (06) :1571-1578
[9]   Insights into Different Photocatalytic Oxidation Activities of Anatase, Brookite, and Rutile Single-Crystal Facets [J].
Guennemann, Carsten ;
Haisch, Christoph ;
Fleisch, Manuel ;
Schneider, Jenny ;
Emeline, Alexei V. ;
Bahnemann, Detlef W. .
ACS CATALYSIS, 2019, 9 (02) :1001-1012
[10]   Review of the anatase to rutile phase transformation [J].
Hanaor, Dorian A. H. ;
Sorrell, Charles C. .
JOURNAL OF MATERIALS SCIENCE, 2011, 46 (04) :855-874