High-Temperature Synthesis of Cast Cr2AlC at an Inert Gas Overpressure

被引:7
|
作者
Miloserdov, P. A. [1 ]
Gorshkov, V. A. [1 ]
Yukhvid, V. I. [1 ]
机构
[1] Russian Acad Sci, Inst Struct Macrokinet & Mat Sci, Chernogolovka 142432, Moscow Oblast, Russia
关键词
Spark Plasma Sinter; Self Propagate High Temperature Synthesis; Combustion Velocity; Chromium Carbide; Self Propagate High Temperature Synthesis Process;
D O I
10.1134/S002016851307011X
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
This paper reports the high-temperature synthesis of cast Cr2AlC from mixtures of chromium(III) oxide, chromium(VI) oxide, aluminum, and carbon at an increased inert gas (Ar or N) pressure in a 3-L self-propagating high-temperature synthesis reactor at an initial argon pressure p(i) = 5 MPa. The reaction products were characterized by X-ray diffraction and X-ray microanalysis. The results indicate that the ingots obtained under optimized conditions consisted of Cr2AlC and Cr3C2 with a ratio of about 85 : 15.
引用
收藏
页码:781 / 785
页数:5
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