Sample pretreatment strategies for total reflection X-ray fluorescence analysis: A tutorial review

被引：115

作者：

De La Calle, I. ^{[1
]}

Cabaleiro, N. ^{[1
]}

Romero, V. ^{[1
]}

Lavilla, I. ^{[1
]}

Bendicho, C. ^{[1
]}

机构：

[1] Univ Vigo, Fac Quim, Area Quim Analit, Dept Quim Analit & Alimentaria, Vigo 36130, Spain

来源：

SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY | 2013年 / 90卷

关键词：

Total reflection X-ray fluorescence; Sample pretreatment; Multielemental analysis; Tutorial review; TRACE-ELEMENT DETERMINATION; SOLID-PHASE EXTRACTION; ATOMIC-ABSORPTION-SPECTROMETRY; GEL-PERMEATION CHROMATOGRAPHY; HEAVY-METAL TRACES; MULTIELEMENTAL ANALYSIS; SYNCHROTRON-RADIATION; WATER SAMPLES; MEMBRANE COMPLEXATION; MERCURY DETERMINATION;

D O I：

10.1016/j.sab.2013.10.001

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

In the last years, there has been a revival of total reflection X-ray fluorescence spectrometry (TXRF), which was firstly applied for analytical purposes in the late 80s. The aim of this work is to discuss and compare the current approaches for sample pretreatment including in situ microdigestion, slurry preparation, acid digestion, extraction, etc. prior to TXRF analysis. Advantages and drawbacks inherent to each of those procedures are considered. A comprehensive revision in the period January 2008-July 2013 about different sample preparation strategies prior to TXRF analysis apart from early pioneering reports dealing with sample pretreatment are included in the review. Non-conventional sample pretreatment approaches such as microflow online preconcentration, lab-on-a-chip, etc., are also discussed. Finally, future prospects in sample preparation prior to TXRF analysis are outlined. (C) 2013 Elsevier B.V. All rights reserved.

引用

页码：23 / 54

页数：32

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