2′-Chloro-4-(1-methyl-1H-imidazol-2-yl)-2,4′-bipyridine

被引：2

作者：

Zinad, Dhafer Saber ^{[1
]}

AL-Duhaidahaw, Dunya L. ^{[2
]}

Al-Amiery, Ahmed ^{[3
]}

机构：

[1] Univ Technol Baghdad, Appl Sci Dept, Baghdad 10001, Iraq

[2] Univ Kufa, Pharmaceut Chem Dept, Coll Pharm, Al Najaf 31001, Iraq

[3] Univ Technol Baghdad, Energy & Renewable Energies Technol Ctr, Baghdad 10001, Iraq

来源：

MOLBANK | 2019年 / 01期

关键词：

Suzuki-Miyaura; imidazole; boronic acid; palladium-catalyzed; mass spectrometry; CROSS-COUPLING REACTIONS; MILD-STEEL CORROSION; ACID-SOLUTION; INHIBITION;

D O I：

10.3390/M1040

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The compound 2-chloro-4-(1-methyl-1H-imidazol-2-yl)-2,4-bipyridine was obtained with a good yield by the reaction of 2-chloro-4-(1-methyl-1H-imidazol-2-yl)pyridine with (2-chloropyridin-4-yl)boronic acid and structurally characterized by nuclear magnetic resonance (H-1-NMR and C-13-NMR), thin-layer chromatography-mass spectrometry (TLC-MS), HPLC, gas chromatography-mass spectrometry (GC-MS), and elemental analysis. The functionalization of the pyridine was achieved by the palladium-catalyzed Suzuki-Miyaura carbon-carbon cross-coupling reaction that afforded the target compound.

引用

页数：4

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