Synthesis of two-dimensional micron-size single-crystalline Prussian blue nanosheets by hydrothermal methods assisted by glucose

被引:21
作者
Pan, Qingtao [1 ]
Huang, Kai [1 ]
Ni, Shibing [1 ]
Yang, Feng [1 ]
He, Deyan [1 ]
机构
[1] Lanzhou Univ, Dept Phys, Lanzhou 730000, Peoples R China
基金
高等学校博士学科点专项科研基金;
关键词
Nanostructures; Chemical synthesis; Electron microscopy; LARGE-SCALE SYNTHESIS; NANOPARTICLES; NANOCOMPOSITES; NANOCLUSTERS; FERRICYANIDE; FABRICATION; TRANSITION; CHEMISTRY; MECHANISM;
D O I
10.1016/j.materresbull.2008.05.007
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Prussian blue Fe-4[Fe(CN)(6)](3) nanosheets have been successfully prepared by a simple hydrothermal process employing the reactions between K-3[Fe(CN)(6)] and glucose (C6H12O6). X-ray diffraction and transmission electron microscopy measurement results show that the Prussian blue nanosheets are highly crystalline with a face-centered-cubic structure of a = 10.26 angstrom. It was found the C6H12O6 is not only a reductant, but also may be a template for synthesizing the nanosheets. (C) 2008 Elsevier Ltd. All rights reserved.
引用
收藏
页码:388 / 392
页数:5
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