Microwave Sintering of Zirconia Materials: Mechanical and Microstructural Properties

被引:56
作者
Borrell, Amparo [1 ]
Salvador, Maria D. [2 ]
Penaranda-Foix, Felipe L. [3 ]
Catala-Civera, Jose M. [3 ]
机构
[1] Univ Oviedo, CSIC, CINN, Llanera 33428, Asturias, Spain
[2] Univ Politecn Valencia, ITM, Valencia 46022, Spain
[3] Univ Politecn Valencia, Inst Aplicac Tecnol Informac & Comunicac Avanzada, Valencia 46022, Spain
关键词
YTTRIA-STABILIZED ZIRCONIA; MOL-PERCENT YTTRIA; GRAIN-GROWTH; CERAMICS; VARISTORS; ALUMINA; FIELD; GHZ;
D O I
10.1111/j.1744-7402.2011.02741.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Commercially, 3mol% Y2O3-stabilized tetragonal zirconia (7090nm) compacts were fabricated using a conventional and a nonconventional sintering technique; microwave heating in a resonant mono-mode cavity at 2.45GHz, at temperatures in the 11001400 degrees C range. A considerable difference in the densification behavior between conventional (CS) and microwave (MW) sintered materials was observed. The MW materials attain a full density of 99.9% of the theoretical density (t.d.) at 1400 degrees C/10min, whereas the CS reach only 98.0% t.d. at the same temperature and 1h of dwelling time. Therefore, the MW materials exhibit superior Vickers hardness values (16.0GPa) when compared with CS (13.4GPa).
引用
收藏
页码:313 / 320
页数:8
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