Improved gas chromatography-mass spectrometry method for the determination of clenbuterol and salbutamol in animal urine

被引：0

作者：

Sniegocki, T ^{[1
]}

Posyniak, A ^{[1
]}

Zmudzki, J ^{[1
]}

机构：

[1] Natl Inst Vet Res, Dept Pharmacol & Toxicol, PL-24100 Pulawy, Poland

来源：

BULLETIN OF THE VETERINARY INSTITUTE IN PULAWY | 2005年 / 49卷 / 04期

关键词：

clenbuterol; salbutamol; residues; urine; gas chromatography;

D O I：

暂无

中图分类号：

S85 [动物医学（兽医学）];

学科分类号：

0906 ;

摘要：

An improved gas chromatography-mass spectrometry method, prepared for the confirmatory purposes, included solid phase extraction, derivatization, and analysis of clenbuterol and salbutamol derivatives. The whole procedure was validated in terms of linearity, decision limit detection capability precision, recovery, and uncertainty. The results of validation indicate that the prepared procedure is suitable for the confirmatory purposes. The decision limit for clenbuterol and salbutamol was established at the level of 0.022 ng/ml and 0.024 ng/ml, respectively, and the recoveries were about 70%.

引用

页码：443 / 447

页数：5

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