The synthesis of amine-capped magnetic (Fe, Mn, Co, Ni) oxide nanocrystals and their surface modification for aqueous dispersibility

被引:92
作者
Li, Yang
Afzaal, Mohammad
O'Brien, Paul
机构
[1] Univ Manchester, Sch Mat, Manchester M13 9PL, Lancs, England
[2] Univ Manchester, Sch Chem, Manchester M13 9PL, Lancs, England
关键词
D O I
10.1039/b517351e
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Nano-dimensional single-crystals of Fe, Mn, Co or Ni oxides have been prepared by the decomposition of their metal acetylacetonate at elevated temperatures in hexadecylamine. The amine acts as both a solvent and the capping agent. The crystalline structure and morphology of resulting samples have been characterized by TEM, HRTEM, SAED and XRD. The nanocrystals can be dispersed in aqueous solution by overcoating the surface with amphiphilic polyelectrolytes.
引用
收藏
页码:2175 / 2180
页数:6
相关论文
共 24 条
[21]   VISCOMETRIC BEHAVIOR OF HYDROPHOBICALLY MODIFIED POLY(SODIUM ACRYLATE) [J].
WANG, KT ;
ILIOPOULOS, I ;
AUDEBERT, R .
POLYMER BULLETIN, 1988, 20 (06) :577-582
[22]   Chemically prepared magnetic nanoparticles [J].
Willard, MA ;
Kurihara, LK ;
Carpenter, EE ;
Calvin, S ;
Harris, VG .
INTERNATIONAL MATERIALS REVIEWS, 2004, 49 (3-4) :125-170
[23]  
Yu WW, 2002, ANGEW CHEM INT EDIT, V41, P2368, DOI 10.1002/1521-3773(20020703)41:13<2368::AID-ANIE2368>3.0.CO
[24]  
2-G