In situ small angle X-ray scattering investigation of ultrasound induced nucleation in a metallic alloy melt

被引:45
作者
Huang, Haijun [1 ]
Shu, Da [1 ]
Zeng, Jianrong [2 ]
Bian, Fenggang [2 ]
Fu, Yanan [2 ]
Wang, Jun [1 ,3 ]
Sun, Baode [1 ,3 ]
机构
[1] Shanghai Jiao Tong Univ, Shanghai Key Lab Adv High Temp Mat & Precis Formi, Shanghai 200240, Peoples R China
[2] Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai Synchrotron Radiat Facil, Shanghai 201204, Peoples R China
[3] Shanghai Jiao Tong Univ, State Key Lab Met Matrix Composites, Shanghai 200240, Peoples R China
基金
美国国家科学基金会;
关键词
Nucleation; SAXS; Ultrasonic; Cavitation; MECHANICAL-PROPERTIES; GRAIN-REFINEMENT; AL-CU; ALUMINUM; GROWTH; SAXS; ICE; NANOPARTICLES; LIQUID;
D O I
10.1016/j.scriptamat.2015.04.011
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
An in situ synchrotron small angle X-ray scattering (SAXS) method was employed to probe the change of scattering structures in an Al-Cu alloy melt after ultrasonic melt treatment. The size distribution and fractal geometry of the scatterers were evaluated by quantitative SAXS analysis. Results show that cavitation induced nuclei on the clusters or impurities, and the remnants, showing bigger sizes and lower surface fractal dimensions in a melt of lower superheating, could preserve grain refining potential for at least 20 min. (C) 2015 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:21 / 25
页数:5
相关论文
共 33 条
  • [1] ACTION OF HIGH-INTENSITY ULTRASOUND ON SOLIDIFYING METAL
    ABRAMOV, OV
    [J]. ULTRASONICS, 1987, 25 (02) : 73 - 82
  • [2] [Anonymous], 1998, Ultrasonic Treatment of Light Alloy Melts
  • [3] Criteria of Grain Refinement Induced by Ultrasonic Melt Treatment of Aluminum Alloys Containing Zr and Ti
    Atamanenko, T. V.
    Eskin, D. G.
    Zhang, L.
    Katgerman, L.
    [J]. METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 2010, 41A (08): : 2056 - 2066
  • [4] Local structure in liquid binary Al-Cu and Al-Ni alloys
    Brillo, J.
    Bytchkov, A.
    Egry, I.
    Hennet, L.
    Mathiak, G.
    Pozdnyakova, I.
    Price, D. L.
    Thiaudiere, D.
    Zanghi, D.
    [J]. JOURNAL OF NON-CRYSTALLINE SOLIDS, 2006, 352 (38-39) : 4008 - 4012
  • [5] The Effect of Ultrasonic Treatment on Microstructural and Mechanical Properties of Cast Magnesium Alloys
    Chen, Yeong-Jern
    Hsu, Wen-Nong
    Shih, Jhih-Ren
    [J]. MATERIALS TRANSACTIONS, 2009, 50 (02) : 401 - 408
  • [6] A study on the primary and secondary nucleation of ice by power ultrasound
    Chow, R
    Blindt, R
    Chivers, R
    Povey, M
    [J]. ULTRASONICS, 2005, 43 (04) : 227 - 230
  • [7] The sonocrystallisation of ice in sucrose solutions: primary and secondary nucleation
    Chow, R
    Blindt, R
    Chivers, R
    Povey, M
    [J]. ULTRASONICS, 2003, 41 (08) : 595 - 604
  • [8] Dahlborg U., 2008, ACTA MAT, V56, P6264
  • [9] Glatter O, 1982, Small angle x-ray scattering
  • [10] Nucleation and Growth of Metal Nanoparticles during Photoreduction Using In Situ Time-Resolved SAXS Analysis
    Harada, Masafumi
    Tamura, Noriko
    Takenaka, Mikihito
    [J]. JOURNAL OF PHYSICAL CHEMISTRY C, 2011, 115 (29) : 14081 - 14092