Controllable growth of SnO2 nanoparticles by citric acid assisted hydrothermal process

被引:65
作者
Li, Zhijie [1 ]
Shen, Wenzhong [2 ]
Zhang, Xue [3 ]
Fang, Limei [1 ]
Zu, Xiaotao [1 ]
机构
[1] Univ Elect Sci & Technol China, Dept Appl Phys, Chengdu 610041, Peoples R China
[2] China Univ Petr, State Key Lab Heavy Oil, Dongying 257061, Peoples R China
[3] Well Tech China Offshore Serv Ltd, Equipment Manufactory, Beijing 101149, Peoples R China
关键词
SnO2; nanoparticles; citric acid; hydrothermal;
D O I
10.1016/j.colsurfa.2008.05.043
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
SnO2 nanoparticles were prepared by citric acid assisted hydrothermal process and its microstructure and optoelectronic properties had been investigated. Based on XRD, TEM and FT-IR analyses, the SnO2 crystallites with the tetragonal rutile structure were directly formed. The crystalline grain size of SnO2 was 6.0nm and its specific surface area reached 206m(2)/g. The room temperature photoluminescence proved that it had a blue emission, which increased remarkably after SnO2 calcined at 800 degrees C. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:17 / 20
页数:4
相关论文
共 31 条
[1]   Influences of ball-milling time on gas-sensing properties Of Co3O4-SnO2 composites [J].
Abe, S ;
Choi, US ;
Shimanoe, K ;
Yamazoe, N .
SENSORS AND ACTUATORS B-CHEMICAL, 2005, 107 (02) :516-522
[2]   Investigation of the structural and electrochemical properties of size-controlled SnO2 nanoparticles [J].
Ahn, HJ ;
Choi, HC ;
Park, KW ;
Kim, SB ;
Sung, YE .
JOURNAL OF PHYSICAL CHEMISTRY B, 2004, 108 (28) :9815-9820
[3]   PHOTOCATALYTIC HYDROGENATION OF CH3CCH WITH H2O ON SMALL-PARTICLE TIO2 - SIZE QUANTIZATION EFFECTS AND REACTION INTERMEDIATES [J].
ANPO, M ;
SHIMA, T ;
KODAMA, S ;
KUBOKAWA, Y .
JOURNAL OF PHYSICAL CHEMISTRY, 1987, 91 (16) :4305-4310
[4]   Synthesis of nanocrystalline SnO2 powder by amorphous citrate route [J].
Bhagwat, M ;
Shah, P ;
Ramaswamy, V .
MATERIALS LETTERS, 2003, 57 (9-10) :1604-1611
[5]   Grain size dependent electrical studies on nanocrystalline SnO2 [J].
Bose, AC ;
Thangadurai, P ;
Ramasamy, S .
MATERIALS CHEMISTRY AND PHYSICS, 2006, 95 (01) :72-78
[6]   Photoelectrochemical behaviour of a dye-grafted nanocrystalline SnO2 powder [J].
Cachet, H ;
Vivier, V ;
Toupance, T .
JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 2004, 572 (02) :249-255
[7]   Novel nanostructures of functional oxides synthesized by thermal evaporation [J].
Dai, ZR ;
Pan, ZW ;
Wang, ZL .
ADVANCED FUNCTIONAL MATERIALS, 2003, 13 (01) :9-24
[8]   In situ diffuse reflectance infrared spectroscopy study of CO adsorption on SnO2 [J].
Emiroglu, S ;
Bârsan, N ;
Weimar, U ;
Hoffmann, V .
THIN SOLID FILMS, 2001, 391 (02) :176-185
[9]   Dye sensitization of nanocrystalline tin oxide by perylene derivatives [J].
Ferrere, S ;
Zaban, A ;
Gregg, BA .
JOURNAL OF PHYSICAL CHEMISTRY B, 1997, 101 (23) :4490-4493
[10]   NO2-gas-sensing properties of mixed In2O3-SnO2 thin films [J].
Forleo, A ;
Francioso, L ;
Epifani, M ;
Capone, S ;
Taurino, AM ;
Siciliano, P .
THIN SOLID FILMS, 2005, 490 (01) :68-73