An expedient synthesis of allylic polyprenyl phosphates

被引：16

作者：

Branch, CL ^{[1
]}

Burton, G ^{[1
]}

Moss, SF ^{[1
]}

机构：

[1] SmithKline Beecham Pharmaceut, Dept Med Chem, Harlow CM19 5AW, Essex, England

来源：

SYNTHETIC COMMUNICATIONS | 1999年 / 29卷 / 15期

关键词：

D O I：

10.1080/00397919908086425

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Allylic polyprenyl phosphates 6c-d have been prepared in high yield from polyprenyl alcohols via an operationally straightforward oxidation and deprotection sequence utilising phosphite triesters 4.

引用

页码：2639 / 2644

页数：6

共 15 条

[1] A SIMPLE AND EFFECTIVE CHEMICAL PHOSPHORYLATION PROCEDURE FOR BIOMOLECULES [J].

BANNWARTH, W ;

TRZECIAK, A .

HELVETICA CHIMICA ACTA, 1987, 70 (01) :175-186

[2]

DANILOV LL, 1984, SYNTHESIS-STUTTGART, P404

[3] POLYPRENYL PHOSPHATES - SYNTHESIS AND STRUCTURE-ACTIVITY RELATIONSHIP FOR A BIOSYNTHETIC SYSTEM OF SALMONELLA-ANATUM O-SPECIFIC POLYSACCHARIDE [J].

DANILOV, LL ;

DRUZHININA, TN ;

KALINCHUK, NA ;

MALTSEV, SD ;

SHIBAEV, VN .

CHEMISTRY AND PHYSICS OF LIPIDS, 1989, 51 (3-4) :191-203

[4] A SIMPLE PROCEDURE FOR PREPARING DOLICHYL MONOPHOSPHATE BY THE USE OF POC13 [J].

DANILOV, LL ;

CHOJNACKI, T .

FEBS LETTERS, 1981, 131 (02) :310-312

[5]

DANILOV LL, 1983, BIOORG KHIM+, V9, P844

[6]

DANILOV LL, 1991, STUDIES NATURAL PROD, V8, P63

[7] A SIMPLE METHOD FOR THE SYNTHESIS OF PRIMARY AND TERTIARY ALLYLIC TERPENIC PHOSPHATES [J].

JULIA, M ;

MESTDAGH, H ;

ROLANDO, C .

TETRAHEDRON, 1986, 42 (14) :3841-3849

[8] NOVEL NONENZYMIC HETEROLYSIS OF AN ALLYL PHOSPHATE ESTER BY ORGANOALUMINUM REAGENTS [J].

KITAGAWA, Y ;

HASHIMOTO, S ;

IEMURA, S ;

YAMAMOTO, H ;

NOZAKI, H .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1976, 98 (16) :5030-5031

[9] MODEL STUDIES ON THE QUINONE-CONTAINING COPPER AMINE OXIDASES - UNAMBIGUOUS DEMONSTRATION OF A TRANSAMINATION MECHANISM [J].

LEE, Y ;

SAYRE, LM .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1995, 117 (48) :11823-11828

[10] NUCLEOTIDE CHEMISTRY .20. PHOSPHITE COUPLING PROCEDURE FOR GENERATING INTERNUCLEOTIDE LINKS [J].

LETSINGER, RL ;

FINNAN, JL ;

HEAVNER, GA ;

LUNSFORD, WB .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (11) :3278-3279

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