Complete H-1 and C-13 NMR assignments of the oligosaccharide antibiotic Sch 27899

被引:0
作者
Chan, TM
Osterman, RM
Morton, JB
Ganguly, AK
机构
关键词
NMR; H-1; C-13; HMQC; HMQC-TOCSY; HMBC; everninomicin;
D O I
10.1002/(SICI)1097-458X(199708)35:8<529::AID-OMR120>3.0.CO;2-7
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The complete assignments of H-1 and C-13 data for Sch 27899 are described. The compound is an oligosaccharide antibiotic belonging to the class everninomicin. It has a molecular mass of 1629. The assignments are based on 2D HMQC, HMQC-TOCSY and HMBC experiments. (C) 1997 by John Wiley & Sons, Ltd.
引用
收藏
页码:529 / 532
页数:4
相关论文
共 8 条
[1]   H-1 AND C-13 ASSIGNMENTS FROM SENSITIVITY-ENHANCED DETECTION OF HETERONUCLEAR MULTIPLE-BOND CONNECTIVITY BY 2D MULTIPLE QUANTUM NMR [J].
BAX, A ;
SUMMERS, MF .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1986, 108 (08) :2093-2094
[2]   SENSITIVITY-ENHANCED TWO-DIMENSIONAL HETERONUCLEAR SHIFT CORRELATION NMR-SPECTROSCOPY [J].
BAX, A ;
SUBRAMANIAN, S .
JOURNAL OF MAGNETIC RESONANCE, 1986, 67 (03) :565-569
[3]   STRUCTURE OF EVERNINOMICIN D [J].
GANGULY, AK ;
SARRE, OZ ;
GREEVES, D ;
MORTON, J .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (07) :1982-1985
[4]  
GANGULY AK, 1989, HETEROCYCLES, V28, P83
[5]  
GIRIJAVALLABHAN VM, 1992, KIRKOTHMER ENCY CHEM, V3, P259
[6]   SENSITIVITY-ENHANCED TWO-DIMENSIONAL HETERONUCLEAR RELAYED COHERENCE TRANSFER NMR-SPECTROSCOPY [J].
LERNER, L ;
BAX, A .
JOURNAL OF MAGNETIC RESONANCE, 1986, 69 (02) :375-380
[7]  
LOEBENBERG D, 1993, 33 INT C ANT AG CHEM, P202
[8]  
Mueller L, 1979, J AM CHEM SOC, V101, P4481