Silica sulfuric acid as an efficient heterogeneous catalyst for the synthesis of 1,1-diacetates under solvent-free conditions

被引:56
作者
Hajipour, AR
Zarei, A
Khazdooz, L
Mirjalili, BBF
Sheikhan, N
Zahmatkesh, S
Ruoho, AE
机构
[1] Univ Wisconsin, Sch Med, Dept Pharmacol, Madison, WI 53706 USA
[2] Isfahan Univ Technol, Coll Chem, Pharmaceut Res Lab, Esfahan 84156, Iran
[3] Yazd Univ, Dept Chem, Coll Sci, Yazd, Iran
来源
SYNTHESIS-STUTTGART | 2005年 / 20期
关键词
silica sulfuric acid; 1,1-diacetate; solvent-free;
D O I
10.1055/s-2005-918416
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
An efficient method for the preparation of acylals from different aldehydes in the presence of silica sulfuric acid and acetic anhydride under solvent-free conditions is reported.
引用
收藏
页码:3644 / 3648
页数:5
相关论文
共 39 条
  • [1] Aggarwal VK, 1998, SYNLETT, P849
  • [2] Bismuth compounds in organic synthesis. Bismuth nitrate catalyzed chemoselective synthesis of acylals from aromatic aldehydes
    Aggen, DH
    Arnold, JN
    Hayes, PD
    Smoter, NJ
    Mohan, RS
    [J]. TETRAHEDRON, 2004, 60 (16) : 3675 - 3679
  • [3] An efficient method for the chemoselective synthesis of acylals from aromatic aldehydes using bismuth triflate
    Carrigan, MD
    Eash, KJ
    Oswald, MC
    Mohan, RS
    [J]. TETRAHEDRON LETTERS, 2001, 42 (46) : 8133 - 8135
  • [4] Chandra KL, 2000, SYNLETT, P359
  • [5] Iodine as acetylation catalyst in the preparation of 1,1-diacetates from aldehydes
    Deka, N
    Kalita, DJ
    Borah, R
    Sarma, JC
    [J]. JOURNAL OF ORGANIC CHEMISTRY, 1997, 62 (05) : 1563 - 1564
  • [6] EANDERSON WR, 1985, Patent No. 125781
  • [7] Aluminum dodecatungstophosphate (AlPW12O40) as an efficient heterogeneous inorganic catalyst for the chemoselective synthesis of geminal diacetates (acylals) under solvent-free conditions
    Firouzabadi, H
    Iranpoor, N
    Nowrouzi, F
    Amani, K
    [J]. TETRAHEDRON LETTERS, 2003, 44 (20) : 3951 - 3954
  • [8] PREPARATION AND SPECTRAL PROPERTIES OF BENZYLIDENE DIACETATES
    FREEMAN, F
    KARCHEFSKI, EM
    [J]. JOURNAL OF CHEMICAL AND ENGINEERING DATA, 1977, 22 (03) : 355 - 357
  • [9] ACETALS AS CROSSLINKING REAGENTS FOR COTTON
    FRICK, JG
    HARPER, RJ
    [J]. JOURNAL OF APPLIED POLYMER SCIENCE, 1984, 29 (04) : 1433 - 1447
  • [10] Indium triflate: a reusable catalyst for expeditious chemoselective conversion of aldehydes to acylals
    Ghosh, R
    Maiti, S
    Chakraborty, A
    Haider, R
    [J]. JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2004, 215 (1-2) : 49 - 53