Silica sulfuric acid as an efficient heterogeneous catalyst for the synthesis of 1,1-diacetates under solvent-free conditions

被引:56
作者
Hajipour, AR
Zarei, A
Khazdooz, L
Mirjalili, BBF
Sheikhan, N
Zahmatkesh, S
Ruoho, AE
机构
[1] Univ Wisconsin, Sch Med, Dept Pharmacol, Madison, WI 53706 USA
[2] Isfahan Univ Technol, Coll Chem, Pharmaceut Res Lab, Esfahan 84156, Iran
[3] Yazd Univ, Dept Chem, Coll Sci, Yazd, Iran
来源
SYNTHESIS-STUTTGART | 2005年 / 20期
关键词
silica sulfuric acid; 1,1-diacetate; solvent-free;
D O I
10.1055/s-2005-918416
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
An efficient method for the preparation of acylals from different aldehydes in the presence of silica sulfuric acid and acetic anhydride under solvent-free conditions is reported.
引用
收藏
页码:3644 / 3648
页数:5
相关论文
共 39 条
[1]  
Aggarwal VK, 1998, SYNLETT, P849
[2]   Bismuth compounds in organic synthesis. Bismuth nitrate catalyzed chemoselective synthesis of acylals from aromatic aldehydes [J].
Aggen, DH ;
Arnold, JN ;
Hayes, PD ;
Smoter, NJ ;
Mohan, RS .
TETRAHEDRON, 2004, 60 (16) :3675-3679
[3]   An efficient method for the chemoselective synthesis of acylals from aromatic aldehydes using bismuth triflate [J].
Carrigan, MD ;
Eash, KJ ;
Oswald, MC ;
Mohan, RS .
TETRAHEDRON LETTERS, 2001, 42 (46) :8133-8135
[4]  
Chandra KL, 2000, SYNLETT, P359
[5]   Iodine as acetylation catalyst in the preparation of 1,1-diacetates from aldehydes [J].
Deka, N ;
Kalita, DJ ;
Borah, R ;
Sarma, JC .
JOURNAL OF ORGANIC CHEMISTRY, 1997, 62 (05) :1563-1564
[6]  
EANDERSON WR, 1985, Patent No. 125781
[7]   Aluminum dodecatungstophosphate (AlPW12O40) as an efficient heterogeneous inorganic catalyst for the chemoselective synthesis of geminal diacetates (acylals) under solvent-free conditions [J].
Firouzabadi, H ;
Iranpoor, N ;
Nowrouzi, F ;
Amani, K .
TETRAHEDRON LETTERS, 2003, 44 (20) :3951-3954
[8]   PREPARATION AND SPECTRAL PROPERTIES OF BENZYLIDENE DIACETATES [J].
FREEMAN, F ;
KARCHEFSKI, EM .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 1977, 22 (03) :355-357
[9]   ACETALS AS CROSSLINKING REAGENTS FOR COTTON [J].
FRICK, JG ;
HARPER, RJ .
JOURNAL OF APPLIED POLYMER SCIENCE, 1984, 29 (04) :1433-1447
[10]   Indium triflate: a reusable catalyst for expeditious chemoselective conversion of aldehydes to acylals [J].
Ghosh, R ;
Maiti, S ;
Chakraborty, A ;
Haider, R .
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2004, 215 (1-2) :49-53